3B Scientific Electron Diffraction Tube D User Manual

3b scientific® physics, Electron diffraction tube d

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3B SCIENTIFIC® PHYSICS



1

Electron Diffraction Tube D

1013885



Instruction sheet

07/13 ALF

1

5

4

7 8 9

11

6

2

R

3

10

1 4-mm sockets for connecting

heater supply

2 2-mm socket for connecting

cathode

3 Internal resistor

4 Filament

5 Cathode

6 Anode

7 4-mm plug for connecting

anode

8 Focussing electrode

9 Polycrystalline graphite

grating

10 Boss

11 Fluorescent screen

1. Safety instructions

Hot cathode tubes are thin-walled, highly

evacuated glass tubes. Treat them carefully as

there is a risk of implosion.

Do not subject the tube to mechanical

stresses.

Do not subject the connection leads to any

tension.

The tube may only be used with tube holder

D (1008507).

If voltage or current is too high or the cathode is

at the wrong temperature, it can lead to the tube

becoming destroyed.

Do not exceed the stated operating parame-

ters.

Only change circuit with power supply

equipment switched off.

Only exchange tubes with power supply

equipment switched off.

When the tube is in operation, the stock of the

tube may get hot.

If necessary, allow the tube to cool before

dismantling.

The compliance with the EC directive on elec-

tromagnetic compatibility is only guaranteed

when using the recommended power supplies.

2. Description

The electron diffraction tube illustrates the wave

nature of electrons by allowing observation of

interference caused by a beam of electrons

passing through a polycrystalline graphite target

on a fluorescent screen (Debye-Scherrer diffrac-

tion). The wavelength of the electrons can be

calculated for various anode voltages from the

radius of the diffracted rings and the distance

between the crystal layers in the graphite. The

tube also confirms the de Broglie hypothesis.
The electron diffraction tube is a highly evacu-

ated tube with an electron gun consisting of a

pure tungsten heater filament and a cylindrical

anode all contained in a clear glass bulb. The

electrons emitted by the heated cathode are

constrained to a narrow beam by an aperture

and are then focussed by means of an electron-

optical system. The resulting tight, monochro-

matic beam then passes through a micro-mesh

nickel grating situated at the aperture of the gun.

Onto this grid, a thin layer of polycrystalline

graphitised carbon has been deposited by va-

porisation. This layer affects the electrons in the

beam much like a diffraction grating. The result

of this diffraction is seen in the form of an image

comprising two concentric rings that become

visible on the fluorescent screen. A spot result-

ing from the undeflected electron beam contin-

ues to be visible at the centre of the rings.

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