Gas & vapour sampling, Sorbent tube features, Sorbent break through – SKC Limited AirChek 3000 Deluxe Pump Step By Step Guide User Manual

Page 15

Advertising
background image

www.skcltd.com

224-G1 Issue D

Page 13

Sorbent Tube Features

Gas & Vapour Sampling

To sample for gases or vapours, especially for
longer periods such as 8 hour TWA, the use
of sorbent tubes is a widely accepted method.
A Sorbent is like a sponge, which soaks up
the molecules of the material being sampled
(which can subsequently be extracted and
analysed). Activated charcoal is the most
commonly used material but it cannot adsorb
every substance, which is why other materials
such as Silica Gel and Tenax are often used.
Once the pollutant has been trapped by a
sorbent tube it then needs to be removed for
analysis. This is achieved using either a solvent
wash or heat, which drives the collected
chemicals off the sorbent and into an analytical
instrument such as a Gas Chromatograph.
Most tubes have two layers of sorbent in them,
the smallest of which (usually situated nearest
the pump) is known as the backup. Analysis
of the backup sorbent reveals whether
breakthrough has occurred (see figure below).
Breakthrough occurs when the main layer of
sorbent (nearest the open end of the tube)
has become flooded with the contaminant
chemicals which then overflow into the backup
layer.
Gas is sampled in one of the two following
ways using a sorbent:
1. Active sampling using pumps and tubes.
2. Passive (or Diffusive) sampling using

badges.

There are many different types of sorbents
and an even larger number of different sorbent
tubes. Each tube is designed and validated
for a specific substance. Sorbent tubes vary
in size from the Standard Charcoal Tube (6 x
70mm) to ''Jumbo Tubes'' (10mm x 110mm)
and they have different separators between
the sorbent beds.

NIOSH approved sealing caps

prevent contamination

High purity glass wool

precise amount for uniform

pressure drop

Glass tube

drawn to very close tolerances

for repeatable results

Backup sorbent layer

detects sample breakthrough

Precision lockspring

holds sorbent layers securely

in place to prevent sample

channeling; allows transporting

without damaging sample

(patented)

Sorbent layer

precisely controlled surface

area, pore size, adsorptive

characteristics, particle size

Foam separator

for uniform pressure drop

Precision sealed tips

permit safe, easy breaking to the

specified opening size

Contaminant

saturates sorbent

leading to

break through

Sorbent Break Through

All contaminant

adsorbed by

sorbent

Advertising