3 setting up application parameters, 4 how to perform a wet application, Warning – BUCHI Wet Digester B-440 User Manual

Page 24

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6 Operation

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B-440 Operation Manual, Version D

6.3

Setting up application parameters

Internal program storage

The B-440 is capable of storing 9 application methods in its program storage.

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Each program has 5 steps with individual parameter pairs of time and temperature.

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Parameter name

Range

Programs

1 – 9

Steps

1 – 5

Temperature

ambient – 600 °C

Time (per "STEP")

0 – 240 minutes

Setting up PROGRAMs and STEPs

Switch "ON" the Wet Digester.

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๗After the bootprocess (੠ 4 seconds) the instrument will be operational.
Select a program via the right "SELECT" button (below "PROGRAM" display).

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Press the left "SELECT" button (below "STEP" display) repeatingly to switch through every

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"TIME" / "TEMP" parameter of each "STEP" in a loop.

๗The "STEP" display shows the selected step (1—5 ).
๗The corresponding "TIME" / "TEMP" display will flash for 10 seconds and switch to "STEP" level 1

without button action.

To change either the heating time or temperature of a step, use the "UP" and "DOWN" buttons

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while the respective display flashes.

๗As soon as the display stops flashing, the value is being stored.

NOTE

Some application methods do not require a full set of 5 steps. To disable a "STEP", set its "TIME "

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to 0.

During a running application, programming is not possible.

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6.4

How to perform a wet application

Digestion fumes can be hazardous and must be neutralized by a Scrubber or a condensate

trap / Scrubber combination. Fumes which may escape during operation must be safely withdrawn by

a fume hood! Wear personal protective equipment, see section 2.5 for general safety information!

!

WARNING

Death or serious poisoning by contact or incorporation of harmful substances and fumes at use.

Before operation, check the instrument for correct assembling

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Rinse condensate trap, hoses and connectors before use

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Before operation inspect sealing surfaces and tubes for good condition and tightness

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Secure all hoses with hose clamps

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Exchange worn out or defective parts immediately

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Only operate the instrument in a fume hood

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Directly withdraw released gases and gaseous substances by a Scrubber

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Dispose of condensate in tubings and glassware safely after use

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Do not inhale digestion fumes

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