Hanna Instruments HI 96742 - Manual

INSTRUCTION MANUAL
HI 96742 HI 96742 HI 96742 HI 96742 HI 96742
Iron LR and
Manganese LR
ISM
w w w . h a n n a i n s t . c o m
Preliminary examination:
Please examine this product carefully. Make sure that the instrument is
not damaged. If any damage occured during shipment, please notify
your Dealer.
Each HI 96742 Ion Selective Meter is supplied complete with:
• Two Sample Cuvettes and Caps
• 9V Battery
• Instruction Manual
Note:
save all packing material until you are sure that the instrument
works correctly. Any defective item must be returned in its original
packing.
For more details about spare parts and accessories
see “Accessories”.
Dear Customer,
Thank you for choosing a Hanna product. This manual will provide you
with the necessary information for the correct use of the instrument. Please
read it carefully before using the meter. If you need additional technical
information, do not hesitate to e-mail us at [email protected].
1. RANGE/GLP/ key: press to change the paramter, press and hold
for three seconds to enter GLP mode. In calibration mode press to edit
the date and time.
2. CAL CHECK key: press to perform the validation of the meter, or
press and hold for three seconds to enter calibration mode.
3. ZERO/CFM key: press to zero the meter prior to measurement, to
confirm edited values or to confirm factory calibration restore.
4. READ/ /TIMER key: In measurement mode, press to make a
measurement, or press and hold for three seconds to start a
pre-programmed countdown prior to measurement. In
GLP mode
press to view the next screen.
5. ON/OFF key: to turn the meter on and off.
6. Liquid Crystal Display (LCD)
7. Cuvette alignment indicator
8. Cuvette holder
DISPLAY ELEMENTS DESCRIPTION:
Functional description:
1. The measuring scheme (lamp, cuvette, detector), appears during
different phases of zero or reading measurement
2. Error messages and warnings
3. The battery icon indicates the charge state of the battery
4. The hourglass appears when an internal check is in progress
5. Status messages
6. The chronometer appears when the reaction timer is running
7. The month, day and date icons appear when a date is displayed
8. Four digit main display
9. Measuring units
10. Four digit secondary display
Light High: There is too much light to perform
a measurement. Please check the preparation of
the zero cuvette.
Light Low: There is not enough light to perform
a measurement. Please check the preparation of
the zero cuvette.
No Light: The instrument cannot adjust the
light level. Please check that the sample does
not contain any debris.
Errors and warnings:
ON ZERO READING:
ON SAMPLE READING:
DURING CALIBRATION PROCEDURE:
OTHER ERRORS AND WARNINGS:
Cap error: Appears when external light enters
in the analysis cell. Assure that the cuvette cap
is present.
Cooling lamp: The instrument waits for the
lamp to cool down.
Battery low: The battery must be replaced
soon.
Dead battery: This indicates that the battery
is dead and must be replaced. Once this
indication is displayed, normal operation of the
instrument will be interrupted. Change the
battery and restart the meter.
Standard Low: The standard reading is less
than expected.
Standard High: The standard reading is higher
than expected.
Inverted cuvettes: The sample and the zero
cuvette are inverted.
Zero: A zero reading was not taken. Follow the
instructions of the measurement procedure for
zeroing the meter.
Under range: A blinking “0.00” indicates that
the sample absorbs less light than the zero
reference. Check the procedure and make sure
you use the same cuvette for reference (zero)
and measurement.
Over Range:
A flashing value of the maximum
concentration indicates an over range condition.
The concentration of the sample is beyond the
programmed range: dilute the sample and
re-run the test.
1• Turn the meter on by pressing ON/OFF.
2• When the beeper sounds briefly and the LCD
displays dashes and “P1” (Iron LR) and “P2”
(Manganese LR) the meter is ready. The code
that appears on the secondary display is the
one of the last selected parameter. If necessary,
press RANGE/GLP/ to change parameter.
The blinking “ZERO” indicates that the
instrument needs to be zeroed first.
3• For Iron LR: Fill one graduated mixing
cylinder up to the 25 mL mark with
deionized water. Add the content of one
packet of HI 93746-0 reagent, close the
cylinder and shake well for 30 seconds. This
is the blank.
Fill a cuvette with 10 mL of the blank up to
the mark and replace the cap.
For Manganese LR: Fill one cuvette with 10
mL of deionized water up to the mark. Add
the content of one packet of HI 93748A-0
Ascorbic acid, replace the cap and shake
gently until completely dissolved. Add 0.2
mL of the HI 93748B-0 Alkaline-cyanide
reagent solution, replace the cap and invert
gently to mix for about 30 seconds. Add 1
mL of the HI 93748C-0 0.1% PAN indicator
solution, replace the cap and shake gently.
4• Place the cuvette into the holder and ensure
that the notch on the cap is positioned
securely into the groove.
5• Press ZERO/CFM and the lamp, cuvette and
detector icons will appear on the display,
depending on the measurement phase.
6• After a few seconds the display will show “-
0.0-” . The meter is now zeroed and ready
for measurement.
7• Remove the cuvette.
8• Add the specific test reagent for each
parameter:
Iron LR: Fill one graduated mixing cylinder
up to the 25 mL mark with the sample.
Add the content of one packet of HI 93746-0
reagent, close the cylinder and shake well
for 30 seconds.
Fill a cuvette with 10 mL of the reacted
sample up to the mark and replace the
cap.
For Manganese LR: Fill one cuvette with 10
mL of sample up to the mark. Add the
content of one packet of HI 93748A-0
Ascorbic acid, replace the cap and shake
gently until completely dissolved. Add 0.2
mL of the HI 93748B-0 Alkaline-cyanide
reagent solution, replace the cap and invert
gently to mix for about 30 seconds. Add 1
mL of the HI 93748C-0 0.1% PAN indicator
solution, replace the cap and shake gently.
9• Replace the cuvette into the holder and
ensure that the notch on the cap is
positioned securely into the groove.
10•Press and hold READ/ /TIMER for three
seconds . The display will show the countdown
prior to measurement. The beeper is playing
a beep at the end of countdown period.
Alternatively, wait for:
Iron LR: 30 seconds
Manganese LR: 2 minutes
Then press READ/ /TIMER.
9-10
Measurement procedure:
Measurement
2
5-6
or
3
Technical specifications:
Range Iron LR 0.00 to 1.60 mg/L
Manganese LR 0 to 300 µ/L
Resolution 0.01 mg/L Iron LR
1 µg/L Manganese LR
Accuracy Iron LR ±0.01 mg/L ±8% of reading @ 25°C
Manganese LR ±2 µg/L ±3% of reading @ 25°C
Typical EMC Dev. ±0.01 mg/L Iron LR
±1 µg/L Manganese LR
Light Source Tungsten lamp
Light Detector Silicon Photocell with narrow band interference
filter @ 525 nm
Method For Iron LR: Adaptation of the TPTZ method. The reaction
between iron and the reagent causes a violet tint in the
sample.
For Manganese LR: Adaptation of the PAN Method. The
reaction between manganese and the reagents causes an
orange tint in the sample.
Environment 0 to 50°C (32 to 122°F);
max 95% RH non-condensing
Battery Type 1 x 9 volt
Auto-Shut off After 10' of non-use in measurement mode;
after 1 hour of non-use in calibration mode;
with last reading reminder.
Dimensions 192 x 104 x 69 mm (7.6 x 4.1 x 2.7”)
Weight 360 g (12.7 oz.).
4
5-6
8