Parr Instrument Series 4560 - Manual (Page 2)

Mini Bench Top Reactors
P a r r I n s t r u m e n t C o m p a n y 2
Table of Contents
Preface
Scope — 3
Related Instructions — 3
Safety Information — 3
General Specifi cations — 3
Electrical Ratings— 3
Explanation of Symbols — 4
Environmental Conditions — 4
Provisions for Lifting and Carrying — 4
Intended Usage — 4
Cleaning & Maintenance — 4
User’s Responsibility — 5
Unpack Carefully — 5
Fixed Head or Removable Head Vessel Design — 6
Flat PTFE Gasket or Self Sealing O-ring Closure — 6
Installation
Pressure and Temperature Limits — 7
Assemble the Reactor — 8
Identify the Valves
Gas Inlet Valve — 9
Gas Release Valve — 9
Liquid Sampling Valve — 9
Other Vessel Head Fittings
Safety Rupture Disc — 10
Type J Thermocouple — 10
Pressure Gage — 10
Heaters — 10
Customer Service
Questions concerning the installation or operation of this instrument
can be answered by the Parr Customer Service Department:
1-309-762-7716 • 1-800-872-7720 • Fax: 1-309-762-9453
E-mail: [email protected] • http://www.parrinst.com
How to Use the Vessel
Removable Vessels — 11
Fixed Head Vessels — 11
Air Motor — 13
Explosion Proof Operation — 14
Periodic Pressure Tests — 15
Accessories
Liners — 15
Spare Parts Kit — 15
General Maintenance Notes — 16
4560 Series Reaction Vessel Parts List
Standard Vessel Fittings — 17
High Temperature Vessel Fittings — 22
Overarm Parts List — 25
Figures
Fixed Head with O-ring — 6
Moveable Head with Flat Gasket — 6
Removable Head Vessel (Standard Temperature) — 19
Air Motor Option — 13
Vessel Closure and Standard Internal Parts — 17
4561 Gas Entrainment Assembly — 20
4563 Gas Entrainment Assembly — 20
Mini Head External Fittings & Parts List — 21
Vessel Closure and Standard Internal Parts — 22
Overarm Diagram — 25
Bomb Support Stand with Fixed Head and 1/8 hp
Stirrer Drive Motor — 26
Bomb Support Stand with Moveable Vessel and 1/4
hp Stirrer Drive Motor — 27