Thermo Fisher Scientific Ion Selective Electrodes Ammonium User Manual

Page 5

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TABLE OF CONTENTS

GENERAL INSTRUCTIONS .......................................................................................................... 1

Required Equipment........................................................................................................................ 1
Required Solutions .......................................................................................................................... 1

GENERAL PREPARATION............................................................................................................ 2

Electrode Preparation ...................................................................................................................... 2
Electrode Slope Check (with standard pH/mV meter).................................................................... 2
Electrode Slope Check (with ion meter) ......................................................................................... 2

MEASUREMENT.............................................................................................................................. 3

Measuring Hints .............................................................................................................................. 3
Sample Requirements...................................................................................................................... 3
Units of Measurement ..................................................................................................................... 3

MEASUREMENT PROCEDURE ................................................................................................... 4

Direct Measurement ........................................................................................................................ 4
Direct Measurement of Ammonium (using a standard pH/mV meter)........................................... 4
Direct Measurement of Ammonium (using an ion meter) .............................................................. 5
Low Level Ammonium Determination (using a standard pH/mV meter) ...................................... 6
Low Level Ammonium Determination (using an ion meter).......................................................... 7

ELECTRODE CHARACTERISTICS............................................................................................. 7

Reproducibility................................................................................................................................ 7
Interference...................................................................................................................................... 7
Temperature Influences................................................................................................................... 8
Electrode Response ......................................................................................................................... 9
Electrode Storage ............................................................................................................................ 9
Detection Limit ............................................................................................................................... 9
pH Effects...................................................................................................................................... 10
Electrode Life................................................................................................................................ 10

ELECTRODE THEORY ................................................................................................................ 10

Electrode Operation ...................................................................................................................... 10

TROUBLESHOOTING .................................................................................................................. 11

Troubleshooting Guide.................................................................................................................. 11
Meter ............................................................................................................................................. 11
Electrodes ...................................................................................................................................... 11
Standard......................................................................................................................................... 12
Sample ........................................................................................................................................... 12
Technique ...................................................................................................................................... 12

TROUBLESHOOTING HINTS..................................................................................................... 13

SPECIFICATIONS.......................................................................................................................... 15

ORDERING INFORMATION....................................................................................................... 15


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