Document Outline

• Table 6-1
  • Calorimeter Control Limit Values in J/g When Benzoic Acid is Used as a Test Sample
  • Table 6-2
    • Calorimeter Control Limit Values in cal/g When Benzoic Acid is Used as a Test Sample
  • Table 6-3
    • Calorimeter Control Limit Values in BTU/lb When Benzoic Acid is Used as a Test Sample
  • Table 8-1
    • 6400 Data File Naming Convention
  • Table 8-2
    • 6400 Calorimeter Run Data Template
  • Table 15-1
    • Factory Default Settings
  • Table 15-2
    • Settings for ISO & BSI Methods
• Preface
  • Scope
  • Related Instructions
  • Purpose
  • Explanation of Symbols
  • Safety Information
  • Intended Usage
  • General Specifications
  • Environmental Conditions
  • Provisions for Lifting and Carrying
  • Cleaning & Maintenance
  • Chapter 1
• Installation
  • Environmental Conditions
  • Swagelok Tube Fittings
  • Required Consumables, Utilities and Power Requirements
  • Electrical Connection
  • Front Panel Meter
  • Water Connection
  • Gas Connection
  • Bomb Exhaust Connections
  • Communication Connections
  • Printer Connections
  • Balance Connections
  • Chapter 2
• Quick Start
  • Initial Fill
  • Quick Start
  • Chapter 3
• Operation
  • Menu System
  • Menu Keys
  • Control Keys
  • Programming
  • Default Settings
  • Sample Preparation
  • Test Process
    • Closing the bomb
    • Cool/Rinse
    • Drain
    • Fill Cycle
    • Pre-Period
    • Bomb Firing
    • Post-Period
  • Chapter 4
• Menu Descriptions
  • Main Menu
  • Calorimeter Operation Menu
    • Temperature vs. Time Plot
    • Temperature Plot Setup Menu
  • Operating Controls Menu
    • Spiking Controls
    • Bomb Rinse Tank Controls
  • Program Information and Control Menu
    • Software & Hardware Info
    • User/Factory Settings
  • Calibration Data and Controls Menu
    • Bomb 1
    • Control Plot Chart Plot
  • Thermochemical Corrections Menu
    • Calculation Factors Menu
    • Net Heat/Dry Heat Factors
  • Data Entry Controls Menu
    • Net Heat Data Entry Controls
    • Auto Sample ID Controls
    • Moisture Data Entry Controls
    • Preweigh Sample ID Controls
  • Reporting Controls Menu
  • Communication Controls Menu
    • Balance Port Communications
    • Balance Port Settings
  • File Management Menu
    • Run Data File Manager
  • Diagnostics Menu
    • Data Logger Controls
    • Data Log Items
    • User Defined Buttons
    • I/O Diagnostics:
  • Chapter 5
• Reports
  • Reports
  • Chapter 6
• Standardizations
  • Standardizing the Calorimeter
  • Standard Materials
  • Automatic Statistical Calculations
  • Chapter 7
• Calculations
  • Calculating the Heat of Combustion
  • General Calculations
  • Thermochemical Corrections
  • ASTM and ISO Methods Differ
  • Thermochemical Calculation Details
  • Acid and Sulfur Corrections
  • ASTM Treatment for Acid and Sulfur
  • ISO Calculations
  • Spiking Samples
  • Conversion to Other Moisture Bases
  • Conversion to Net Heat of Combustion
  • Chapter 8
• Computer Communications
  • Computer Connections
  • Samba Server Feature (Optional)
  • Bar Code Port
  • Chapter 9
• Memory Management
  • Clearing Memory
  • Removable SD Memory
  • Chapter 10
• Maintenance
  • Inspection of Critical Sealing Surfaces
  • Bomb Removal
  • Fuses
  • Daily Maintenance
  • Quarterly Maintenance
  • 50 to 100 Test Maintenance
  • 500 Test Maintenance
  • 5000 Test Maintenance
  • 6400 Maintenance Checklist
  • Chapter 11
• Troubleshooting
  • Bomb Exhaust Troubleshooting
  • Jacket Temperature Troubleshooting
  • Error List
  • Chapter 12
• Technical Service
  • Return for Repair
  • Chapter 13
• Parts Lists
  • Principal Assemblies in Calorimeter
  • A1250DD2 Controller Assembly
  • A1265DD Bucket and Stirrer Tube Assembly
  • A1255DD Bucket Stirrer Assembly
  • A1266DD Cover Assembly
  • A1457DD Accessory/Installation Kit
  • Chapter 14
• Drawings
  • 1138 Parts Diagram Key
  • Chapter 15
• Tables
• Figure 1-1
  • Swagelok Tube Fittings
    • Figure 1-2
  • 6400 Calorimeter Back Panel
    • Figure 1-3
  • 6400 External Plumbing
    • Figure 1-4
  • 6400 Calorimeter Peripherals
    • Figure 1-5
  • Multiple Alternate Configurations
    • Figure 3-1
  • Volatile Sample Technique
    • Figure 3-2
  • Cotton Thread Assembly
    • Figure 3-3
  • Bucket Fill Flow Diagram
    • Figure 3-4
  • Pre-Period/Post-Period Flow Diagram
    • Figure 3-5
  • Rinse & Cool Flow Diagram
    • Figure 3-6
  • Drain Flow Diagram
    • Figure 14-1
  • 1138 Parts Diagram
    • Figure 14-2
  • 6400 Cutaway Right
    • Figure 14-3
  • 6400 Cutaway Left
    • Figure 14-4
  • 6400 Cover Open
    • Figure 14-5
  • A1250DD2 Control Schematic
    • Figure 14-6
  • A1251DD Oxygen Solenoid Assembly
    • Figure 14-7
  • A1447DD Water Solenoid Assembly
    • Figure 14-8
  • A1456DD Rinse Valve Assembly
    • Figure 14-9
  • 6400 Internal Plumbing Diagram
    • Figure 14-10
  • 6400 Water Tank and Jacket Cooling Solenoid
    • Figure 14-11
  • A1455DD Propeller Assembly
    • Figure 14-12
  • A1448DD Temperature Control Assembly
    • Figure 14-13
  • A1268DD Stirrer Motor and Mount
    • Figure 14-14
  • 6400 Bucket Assembly
    • Figure 14-15
  • 6400 Air Can Assembly, Cutaway Left
    • Figure 14-16
  • 6400 Air Can Assembly, Cutaway Front
    • Figure 14-17
  • A1450DD Bomb Head Assembly, View 1
    • Figure 14-18
  • A1450DD Bomb Head Assembly, View 2
    • Figure 14-19
  • A1050DD Rinse Collection Assembly
    • Figure 14-20
  • Wiring Diagram
    • Figure 14-21
  • Wiring Diagram
    • Figure 14-22
  • Fuse Diagram