Welch Vacuum 2581B-50 WOB-L Pinston Pump User Manual

Page 8

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8

2.30 Traps

2.31 The need for a Trap

The pumps will handle humid air. All wetted aluminum parts are treated for corrosion protection from

moisture. All other wetted parts are stainless steel. If there is a chance liquid may be drawn from the

process under evacuation, Welch recommends a liquid trap be placed between the process and the pump.

A simple liquid trap is a filtering flask.

When a heavy load of water vapor is evolved from the vacuum process, a cold trap is recommended to

help prevent damage to the pump mechanism. The cold trap, immersed in a suitable Dewar flask, is

installed so that the water vapor may come in contact with the surfaces of the trap and condense.

Commonly used refrigerants are liquid nitrogen or dry ice and acetone or alcohol. Dry ice provides

sufficient cooling to freeze out most heavy water vapor loads. A variety of cold traps are available from

Welch.

The symptom of a high water vapor load is if you have droplets coming out of the exhaust port. If you

see droplets of water, Welch recommends you use a cold trap to capture the water before entering the

pump or dilute the water vapor stream by adding dry nitrogen to the gas flow. Please call our customer

service department for additional information at (847) 676-8800 Ext. 1.

2.32 The care of a Trap

When using a cold trap the refrigerant should be maintained at a high level in the flask to keep the trap

at a uniformly low temperature. If the trap is re-warmed it may allow re-evaporation of the

ondensate. The refrigerant add tube on the liquid nitrogen trap should not be obstructed as the

refrigerant boil-off can produce dangerously high pressures. If the trap becomes saturated it should be

disconnected from the system, drained and cleaned. An increase in pressure in the vacuum system will

normally indicate that the trap has become saturated. To clean the trap, remove the trap from the system

and allow the trap to warm up and rinse off the condensate with a suitable solvent in a fume hood.

Thoroughly clean and dry the trap before reinstalling into the system.

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