Metrohm 930 Compact IC Flex ChS/PP/Deg User Manual

Page 6

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Table of contents

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IV

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930 Compact IC Flex ChS/PP/Deg (2.930.1360)

3.12.2

Mode of operation for the peristaltic pump ........................... 41

3.13 Installing the detector ........................................................ 42

3.14 Connecting the sample degasser (optional) ..................... 43

3.15 Connecting the instrument to a computer ....................... 45

3.16 Connecting the instrument to the power supply ............. 46

3.17 Initial start-up ..................................................................... 47

3.18 Connecting and rinsing the guard column ....................... 49

3.19 Connecting the separation column ................................... 51

3.20 Conditioning ........................................................................ 55

4 Operation

57

5 Operation and maintenance

58

5.1

IC system ............................................................................. 58

5.1.1

Operation .............................................................................. 58

5.1.2

Care ...................................................................................... 58

5.1.3

Maintenance by Metrohm Service .......................................... 58

5.1.4

Shutting down and starting back up ...................................... 59

5.2

Capillary connections ......................................................... 60

5.3

Servicing the door .............................................................. 60

5.4

Handling the eluent ............................................................ 60

5.4.1

Manufacturing eluent ............................................................ 61

5.4.2

Changing the eluent .............................................................. 61

5.5

Servicing the eluent degasser ........................................... 62

5.6

Notes on operating the high-pressure pump ................... 62

5.7

Servicing the high-pressure pump .................................... 63

5.8

Servicing the inline filter .................................................... 76

5.9

Servicing the pulsation absorber ...................................... 79

5.10 Injection valve ..................................................................... 79

5.11 Suppressor .......................................................................... 79
5.11.1

Notes for operating the suppressor ........................................ 79

5.11.2

Taking care of the suppressor housing ................................... 80

5.11.3

Servicing the suppressor ........................................................ 80

5.12 Peristaltic pump .................................................................. 87
5.12.1

Notes on operating the peristaltic pump ................................ 87

5.12.2

Servicing the peristaltic pump ................................................ 87

5.13 Servicing the detector ........................................................ 89

5.14 Rinsing the sample path .................................................... 89

5.15 Separation column ............................................................. 90
5.15.1

Separating efficiency .............................................................. 90

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