Document Outline

• Contents
• 1 About this document
  • 1.1 Warning notices in this document
  • 1.2 Symbols
    • 1.2.1 Warning symbols
    • 1.2.2 Mandatory directive symbols
    • 1.2.3 Other symbols
  • 1.3 Available languages
  • 1.4 Trademarks
• 2 Safety
  • 2.1 Intended use
  • 2.2 Use other than that intended
  • 2.3 Staff qualification
  • 2.4 Residual risks
    • 2.4.1 Dangerous vapors
    • 2.4.2 High internal pressure
    • 2.4.3 Hot surfaces and liquids
    • 2.4.4 Glass breakage
    • 2.4.5 Rotating parts
    • 2.4.6 Faults during operation
  • 2.5 Personal protective equipment
  • 2.6 Modifications
• 3 Product description
  • 3.1 Description of function
  • 3.2 Configuration
    • 3.2.1 Front view
    • 3.2.2 Rear view
    • 3.2.3 Heating bath user interface
    • 3.2.4 Typical application
    • 3.2.5 Type plate
    • 3.2.6 Warning symbols on the device
  • 3.3 Specifications supplied
  • 3.4 Technical data
    • 3.4.1 Rotavapor® R-100
    • 3.4.2 Heating bath B-100
    • 3.4.3 Ambient conditions
    • 3.4.4 Materials
  • 3.5 Safety features
    • 3.5.1 Overheat cut-out
    • 3.5.2 Protection against electrical overload
    • 3.5.3 Clips and holders
    • 3.5.4 Glassware
    • 3.5.5 Optional accessories
• 4 Transport and storage
  • 4.1 Transport
  • 4.2 Storage
• 5 Installation
  • 5.1 Installation site
  • 5.2 Mounting the rotary drive unit
  • 5.3 Fitting the vapor duct and condenser
  • 5.4 Fitting the glass stopcock
  • 5.5 Connecting the vacuum and cooling media tubing
  • 5.6 Electrical connections
  • 5.7 Overview of connections
  • 5.8 Setting up and filling the heating bath
  • 5.9 Quick check
• 6 Operation
  • 6.1 Preparations
    • 6.1.1 Preparing the heating bath
    • 6.1.2 Fitting the evaporating flask
    • 6.1.3 Adjusting immersion angle of evaporating flask
    • 6.1.4 Fitting the receiving flask
    • 6.1.5 Vertical adjustment
      • 6.1.5.1 Moving the vertical adjustment range up/down
  • 6.2 Performing distillation
    • 6.2.1 Raising and lowering the evaporating flask
    • 6.2.2 Adjusting distillation conditions
    • 6.2.3 Optimization distillation
    • 6.2.4 Feeding solvent during distillation
  • 6.3 Finishing distillation
    • 6.3.1 Removing the evaporating flask
    • 6.3.2 Removing the receiving flask
• 7 Cleaning and servicing
  • 7.1 Inspecting and cleaning the vapor duct
  • 7.2 Checking the system for leaks
  • 7.3 Checking seals
  • 7.4 Cleaning the condenser
  • 7.5 Cleaning the heating bath
  • 7.6 Removing solvent accumulations
• 8 Help with faults
  • 8.1 Faults, possible causes and remedies
  • 8.2 Remedy
    • 8.2.1 Resetting overheat safety cut-out
    • 8.2.2 Replacing the fuse
• 9 Taking out of service and disposal
  • 9.1 Taking out of service
  • 9.2 Disposal
• 10 Appendix
  • 10.1 Solvent table
  • 10.2 Spare parts and accessories
    • 10.2.1 Glass apparatus V
    • 10.2.2 Glass apparatus C
    • 10.2.3 Accessories
      • 10.2.3.1 Heating Bath
      • 10.2.3.2 Accessories for heating bath
      • 10.2.3.3 Tubing
      • 10.2.3.4 Further accessories
      • 10.2.3.5 Glassware
    • 10.2.4 Wear parts
      • 10.2.4.1 Vacuum gaskets
      • 10.2.4.2 Seals
      • 10.2.4.3 Hose barbs
      • 10.2.4.4 Further wear parts
    • 10.2.5 Spare parts
  • 10.3 List of abbreviations
  • 10.4 Health and safety approval
  • 10.5 Health and safety