Appendix e - calibration procedures, Appendix e, Calibration procedures – Brookfield DV-III Rheometer User Manual

Page 67

Advertising
background image

Brookfield Engineering Laboratories, Inc.

Page 67

Manual No. M/98-211-A0701

APPENDIX E - Calibration Procedures

The accuracy of the DV-III+ is verified using viscosity standard fluids which are available from
Brookfield Engineering Laboratories or your local Brookfield agent. Viscosity standards are Newtonian,
and therefore, have the same viscosity regardless of spindle speed (or shear rate). Viscosity standards,
calibrated at 25

°

C, are shown in Table E1.

Container size:

For Viscosity Standards < 30,000 cP, use a 600 ml Low Form Griffin Beaker
having a working volume of 500 ml.

For Viscosity Standards

30,000 cP, use the fluid container.

Inside Diameter: 3.25"(8.25cm)
Height:

4.75"(12.1cm)

Note: Container may be larger, but may not be smaller.

Temperature:

As stated on the fluid standard label: (

+

/-) 0.1

°

C

Conditions:

The DV-III+ should be set according to the operating instructions. The water
bath should be stabilized at test temperature. Rheometers with the letters “LV”
or “RV” in the model designation should have the guard leg attached.

Table E1

Normal 25

°

C Standard Fluids

High Temperature Standard Fluids

Viscosity (cP)

Viscosity (cP)

Three Viscosity/Temperatures**

5

5,000

HT-30,000

10

12,500

HT-60,000

50

30,000

HT-100,000

100

60,000

500

100,000

**25

°

C, 93.3

°

C, 149

°

C

1,000

Refer to Brookfield catalog for more
information.

Table E2

MINERAL OIL VISCOSITY STANDARD FLUIDS

BEL Part No.

Viscosity (cP) 25

°

C

B31

31

B210

210

B750

750

B1400

1,400

B2000

2,000

B11000

11,000

B20000

20,000

B80000

80,000

B200000

200,000

B420000

420,000

Advertising