Document Outline

• DuMaster D-480 Bedienungsanleitung.pdf
  • General
    • Revision history
    • About this document
    • Display conventions
    • General information on the operating instructions
  • Basic security settings
    • Working with the operating instructions
    • Representation of safety instructions
    • Instructions for disposal of consumables
    • Intended use of the instrument
    • Warning: residual risks
    • Safety devices in the analyzer
    • Warning signs on the analyzer
    • Warning: changes to the instrument
    • Warning: unsuitable spare parts and consumables
    • Required user knowledge and skills
    • Required personal safety equipment
    • Warning notes during operation
  • Product description
    • Analytical characteristics and technical specifications
      • Analytical characteristics
      • Technical specifications
    • Instrument design
      • Front view
      • Furnace section
      • Rear view
      • Right side view
      • Left side view
      • Top view
      • Peripherals and their function
  • Understanding the instrument and planning its use
    • Layout and mode of functioning
      • Functional units
      • The thermal conductivity detector (TCD)
    • Processes in the instrument during a measurement
      • Sample insertion and initiation of measurement
      • Substance digestion and preparation of the reaction gas mixture
      • Detection of measuring components and evaluation of the measuring signal
      • Formula for determining element concentration of analysis samples(Solids)
    • Basic facts about working with the instrument
      • Setting device parameters
      • Instrument equipment
      • Background knowledge required for calibration
      • Calibration curve calculation method criteria
      • Calibration formulae
      • Routine measuring work
      • Formulae for blank value determination and compensation
      • Formula for determining the daily factor
    • Understanding the operating software
      • Basic functions of the operating software
      • Software user interface
      • Sample view
      • Combi view
      • Status view
      • Right mouse button function
    • Data administration and data security
      • Laboratory information and management system (LIMS)
      • Conditions for operating the LIMS
      • 21 CFR Part 11 functionality
      • Versioning
      • Linking the analyzer and software
  • Work performed by the system administrator
    • Installing and updating the software
    • Configure analyzer
      • What can you modify in the configuration?
      • Defining logon timeout
      • Creating new sections
    • Defining LIMS export settings
      • LIMS export settings
    • Setting up user administration
      • User administration
      • Recommendations for user administration
      • Granting authorizations
    • Defining interfaces
      • Defining the analyzer / PC interface
      • Defining the LIMS / PC interface
      • Defining the balance / PC interface
    • Editing analysis data
      • When does it make sense to edit analysis data?
      • Limits for modifying analysis data
      • Consequences of modifying analysis data
    • Performing checks
      • Checking documents for authenticity
      • Signing documents
      • Viewing the logbook
    • Working with the database
      • Database
      • Administrative work on the database
      • Defining the autoexport directory
      • Database backup
      • Starting the database backup
      • Reorganize database
      • Reloading an old database file
    • Ways of optimizing the use of the analyzer
      • Optimizing basic instrument settings
      • Optimizing sample data editing
      • "Balance" weighing data input program
      • Optimizing data evaluation
    • Performing other administrator tasks
      • Modifying the registration
      • Printer setup
  • Starting up and shutting down the instrument
    • Setting up and starting up the instrument
      • Rules for first-time start-up
      • Instructions for operating the furnace
      • Installation site requirements
      • Gases and chemicals to be provided
      • Start-up
      • Connecting peripherals
      • Connecting supply lines and waste gas lines
      • Removing the transport protection
      • Switching on
      • Default instrument settings
    • Shutting down the instrument
      • Shutting the instrument down for short measuring breaks (standby)
      • Shutting the instrument down for long measuring breaks (switching off)
  • Heating up the furnace / checking parameters
  • Using the instrument
    • Measurement settings
      • Defining keywords for blank and conditioning samples
      • Viewing list of defined factor, monitor and standard samples
      • Defining custom standard substances
      • Defining standard substances as factor and monitor samples
      • Defining standard substances as calibration samples
      • Specifying the computation method for blank value and daily factor
      • Enabling/disabling acoustic signals
      • Configuring error handling
    • Preparing samples
      • Sample preparation instructions
      • Determining sample weight
      • Showing or hiding the weight window
      • Packing samples
    • Preparing measurement work
      • Software usage rules
      • Starting the operating software
      • Showing or hiding the toolbar
      • Waking up the instrument
      • Selecting the operating mode
      • Viewing method settings
      • Defining custom methods
      • Defining the Kjeldahl factor
      • Copy methods
      • Settings for sample input
      • Importing weighing data
      • Prioritizing urgent samples
      • Optimizing sleep and wake-up behavior
    • Performing measurement work
      • Values for oxygen dosing
      • Performing measurements
      • Performing routine measuring work
      • Checklist for blank value / conditioning and daily factor measurements
      • Checklist for real sample measurement
      • Types of blank value determination and their settings
      • Determining blank values
      • Determining the daily factor
      • Stopping continuous analysis
    • Preparing measuring data for evaluation
      • Configuring the sample view
      • Determine measuring units and number of decimal places.
      • Saving the sample view
      • Loading a sample view
      • Configure statistics view
      • Generating statistical data
      • Formulae for generating statistical data
      • Manual peak integration
      • Configuring the graph view
      • Setting the size of the graph
      • Configure report
      • Display print preview
      • Data backup and printing
      • Overview of export and import file formats
      • Exporting analysis data to MS Excel and viewing
      • Exporting LIMS data
    • Working with documents
      • Creating new documents
      • Editing documents
      • Deleting documents
      • Finding documents
      • Copying documents via the clipboard
      • Importing documents
      • Signing documents
      • Checking documents for authenticity
  • Maintaining the instrument
    • Important information about maintenance
      • Maintenance work to be performed by the customer
      • Viewing the status of maintenance intervals
      • Defining maintenance intervals in the software
      • Installing used tubes
      • Preparing and following up maintenance work
      • Conditioning newly installed tubes
    • Performing the calibration
      • Viewing list of defined factor, monitor and standard samples
      • Defining standard substances
      • Viewing calibration coefficients
      • Optimizing instrument condition for calibration
      • Performing the calibration
      • Assessing the calibration curves
    • Calibration tables
      • Calibration table for nitrogen calibration
    • Replacing the ash crucible
      • Purpose and frequency of crucible replacement
      • Removing the ash crucible
      • Installing the ash crucible
    • Replacing sealing elements
      • When to replace sealing elements
      • Removing sealing elements from grooves
    • Ball valve maintenance
      • Removing and dismantling the ball valve
      • Cleaning, assembling and installing the ball valve.
    • Maintaining the Ni flap and the O2 lance
      • Purpose and frequency of maintaining the Ni flap and O2 lance
      • Removing and cleaning the Ni flap
      • Installing the Ni flap
      • Removing, cleaning and re-installing the O2 lance
    • Removing, cleaning and installing the quartz glass bridge
      • Removing the quartz glass bridge
      • Cleaning and installing the quartz glass bridge
    • Removing, cleaning and installing the carousel
      • Removing, cleaning and installing the carousel
    • Emptying and filling reaction tubes
      • Emptying reaction tubes
      • Filling the combustion tube
      • Filling the post combustion tube
      • Filling the reduction tube
    • Removing/installing and conditioning the reaction tubes
      • Removing the reaction tubes from the furnace
      • Installing reaction tubes in the furnace and conditioning
    • Filling, removing and installing the absorption and drying tubes
      • Filling the drying tubes
      • Removing and installing the drying tubes
  • Repairing the instrument
    • Interpreting PC error messages
    • Performing a system test
    • Performing a leak test
    • Leak test procedure
    • Replacing fuses
    • What to do after a computer crash
    • Reacting to a power failure
    • Stopping continuous analysis
    • Re-weighing after sample loss
    • Changing the position of the carousel
    • Export analysis data for support
  • Menu and dialog descriptions
    • Dialog descriptions key
    • File menu
      • File > New (Command)
      • Select document name (Dialog)
      • Select version (Dialog)
      • Save file as (Dialog)
      • File > Delete (Command)
      • Comment modification (Dialog)
      • Sign (Dialog)
      • Verify digital signature (Dialog)
      • Export to LIMS (Dialog)
      • Export peak graphics (Dialog)
      • Configure report (Dialog)
      • Print (Dialog)
      • Print preview (Dialog)
      • Printer setup (Dialog)
      • Open (Dialog)
      • Load balance file (Dialog)
      • Configure backup (Dialog)
      • Clean database (Dialog)
      • Restore database (Dialog)
      • Log in as (Dialog)
      • File > Logoff (Command)
      • File > Exit (Command)
      • File > Export/Import > Create Excel sheet (Command)
    • Edit menu
      • Edit > Redo (Command)
      • Edit > Undo (Command)
      • Edit > Cut (Command)
      • Edit > Copy (Command)
      • Edit > Paste (Command)
      • Edit > Insert line (Command)
      • Edit > Delete line (Command)
      • Swap samples (Dialog)
      • Edit > Modify (Command)
      • Set stop tag (Dialog)
      • Select current sample (Dialog)
      • Set current weighed sample (Dialog)
      • Edit > Update hole positions (Command)
    • View menu
      • View > Toggle (Command)
      • Zoom in/out (Dialog)
      • Configure view (Dialog)
      • Column properties (Dialog)
      • Save views (Dialog)
      • Load views (Dialog)
      • Delete views (Dialog)
      • View > Gridview > Auto align (Command)
      • Configure graph view (Dialog)
      • View > Gaphic > Auto align (Command)
      • Configure statistics view (Dialog)
      • View > Statistic > Auto align (Command)
      • Select columns (Dialog)
    • System menu
      • System > Auto run (Command)
      • System > Single run (Command)
      • System > Stop (Command)
      • System > Auto zero (Command)
      • System > Wake up (Command)
      • Feeding (Dialog)
      • Adjust carousel position (Dialog)
      • Analysis mode (Dialog)
    • Windows menu
      • Windows > Toolbar / Run-Bar (Command)
      • Toolbar
      • Windows > Recent sample (Command)
      • Windows > Status view (Command)
      • Weighing window (Dialog)
      • Windows > Default layout (Command)
    • Options menu
      • Maintenance intervals (Dialog)
      • Replace part (Dialog)
      • Commands for the maintenance of the liquid sampler VLS
      • Leak test (Dialog)
      • Leak test: Test phases (Dialog)
      • System test (Dialog)
      • Error buffer (Dialog)
      • Error display (Dialog)
      • Options > Diagnostics > Baseline recording (Command)
      • Input options (Dialog)
      • Standard samples (Dialog)
      • Keywords (Dialog)
      • Acoustic signals (Dialog)
      • Configure Calculations (Dialog)
      • LIMS settings (Dialog)
      • Device parameters (Dialog)
      • Method (Dialog)
      • Error handling (Dialog)
      • Sleep / wake-up function (Dialog)
      • Monthly logbook (Dialog)
      • Select period (Dialog)
      • Device configuration (Dialog)
      • Configure key value (Dialog)
    • Math menu
      • Math > Blank values > Calculate (Command)
      • Blank values (Dialog)
      • Math. > Factor (Command)
      • Define type of peak (Dialog)
      • Define peak start / end (Dialog)
      • Area assignment (Dialog)
      • Standard samples display (Dialog)
      • Math. > Recalculate (Command)
    • Statistics menu
      • Statistics > Via names (Command)
      • Statistics > Group (Command)
      • Statistics > Sort group (Command)
      • Statistics > Delete group (Command)
      • Statistics > Clear statistic (Command)
      • Statistics > Include/Exclude sample (Command)
      • Statistics > Include/Exclude value (Command)
    • Calibration menu
      • Calibration coefficients (Dialog)
      • Configure calibration (Dialog)
      • Specify lower and upper calibration range (Dialog)
      • Calibration > Next sample (Command)
      • Calibration > Previous sample (Command)
      • Calibration > Next (Command)
      • Calibration > Previous (Command)
    • Help menu
      • Help > Content (Command)
      • Help > Find (Command)
      • Help > BÜCHI Labortechnik AG on the WEB (Command)
      • Product registration (Dialog)
      • Help > About DuMaster (Command)
  • Appendix
    • Warranty
      • Warranty of the overall instrument
      • Warranty on the furnace
    • Accessories, spare parts and consumables
      • Smallest workable unit
      • Required accessories
      • Optional accessories
  • Index
  • Word-Lesezeichen
    • O_4326
    • O_4266
    • O_55
    • O_108
    • O_4262
    • O_4264
    • O_110
    • O_4269
    • O_233
    • O_234
    • O_235
    • O_242
    • O_4270
    • O_4272
    • O_4273
    • O_4334
    • O_4333
    • O_247
    • O_250
    • O_723
    • O_724
    • O_248
    • O_249
    • O_251
    • O_4274
    • O_4275
    • O_4276
    • O_3613
    • O_238
    • O_239
    • O_489
    • O_490
    • O_3614
    • O_3615
    • O_495
    • O_4277
    • O_4324
    • O_3618
    • O_3619
    • O_3620
    • O_4335
    • O_4336
    • O_499
    • O_3484
    • O_3630
    • O_3624
    • O_2077
    • O_3625
    • O_3626
    • O_3627
    • O_1089
    • O_1090
    • O_458
    • O_465
    • O_3631
    • O_3632
    • O_1013
    • O_1022
    • O_1029
    • O_1014
    • O_1023
    • O_1030
    • O_1016
    • O_1024
    • O_1031
    • O_1017
    • O_1025
    • O_1034
    • O_1018
    • O_1026
    • O_1033
    • O_1019
    • O_1894
    • O_1027
    • O_1426
    • O_1032
    • H_1378
    • H_1377
    • H_1379
    • O_3633
    • O_601
    • O_3634
    • O_3635
    • H_1428
    • O_3636
    • H_1925
    • O_3637
    • O_1042
    • O_586
    • O_3638
    • O_3639
    • O_3646
    • O_459
    • O_460
    • O_461
    • O_462
    • O_463
    • O_604
    • O_2036
    • O_606
    • O_607
    • O_608
    • O_609
    • O_3647
    • O_2101
    • O_1060
    • O_1063
    • O_610
    • O_611
    • O_618
    • O_2287
    • O_4332
    • O_4279
    • H_1380
    • H_753
    • H_754
    • O_3649
    • O_3650
    • O_625
    • O_626
    • O_623
    • O_624
    • O_627
    • O_628
    • O_3651
    • O_3652
    • O_3653
    • O_4281
    • O_3656
    • O_4266_1
    • O_636
    • O_637
    • O_638
    • O_4331
    • O_642
    • O_643
    • O_644
    • O_493
    • O_494
    • O_645
    • O_646
    • O_648
    • O_649
    • O_4282
    • O_651
    • O_653
    • O_4283
    • O_655
    • O_656
    • O_657
    • O_658
    • O_660
    • O_1445
    • O_661
    • O_662
    • O_663
    • O_664
    • O_665
    • O_666
    • O_667
    • O_668
    • O_669
    • O_613
    • O_614
    • O_670
    • O_615
    • O_672
    • H_789
    • O_673
    • O_675
    • H_788
    • O_676
    • O_677
    • H_771
    • O_2652
    • H_765
    • H_766
    • O_4284
    • O_679
    • H_736
    • H_737
    • O_680
    • O_4285
    • O_682
    • O_4286
    • O_4288
    • O_4289
    • O_508
    • O_3657
    • O_3658
    • O_3659
    • H_542
    • H_543
    • H_544
    • H_3509
    • H_3660
    • H_546
    • H_559
    • H_778
    • H_779
    • O_2143
    • O_1451
    • O_3661
    • O_3662
    • O_4290
    • O_3663
    • O_4312
    • O_3666
    • O_2658
    • H_900
    • O_3667
    • O_4291
    • O_563
    • O_564
    • O_3514
    • O_457
    • O_565
    • O_566
    • O_567
    • O_3668
    • O_569
    • O_570
    • O_571
    • O_572
    • O_573
    • O_862
    • O_3669
    • O_3670
    • O_1469
    • O_3671
    • O_574
    • O_575
    • O_576
    • O_577
    • O_579
    • O_578
    • O_580
    • O_581
    • O_2385
    • O_414
    • O_582
    • O_1107
    • O_583
    • O_584
    • O_585
    • O_3672
    • O_3673
    • O_3674
    • H_1929
    • H_1928
    • H_2449
    • O_3676
    • O_3677
    • O_3678
    • O_3680
    • O_2697
    • O_688
    • O_3681
    • O_690
    • O_691
    • O_692
    • O_693
    • O_694
    • O_695
    • O_696
    • O_701
    • O_698
    • O_699
    • O_700
    • O_702
    • O_453
    • O_454
    • O_455
    • O_456
    • O_703
    • O_705
    • O_704
    • O_706
    • O_707
    • O_708
    • O_4292
    • O_710
    • O_711
    • O_713
    • O_714
    • O_715
    • H_764
    • O_716
    • O_717
    • O_718
    • O_719
    • O_667_1
    • O_721
    • O_4293
    • O_4294
    • O_3683
    • H_1935
    • H_1936
    • H_3510
    • H_785
    • O_391
    • O_392
    • O_393
    • O_394
    • O_3684
    • O_3685
    • O_4295
    • O_2802
    • O_1857
    • O_720
    • O_3686
    • H_3507
    • O_3691
    • H_1944
    • H_3675
    • H_2440
    • H_824
    • O_827
    • H_826
    • O_3692
    • O_3654
    • O_4296
    • O_3693
    • O_4297
    • O_3532
    • O_3695
    • H_3698
    • O_3700
    • O_3696
    • H_3697
    • H_3508
    • O_4298
    • O_3701
    • O_880
    • O_397
    • O_399
    • O_4299
    • O_3721
    • O_3722
    • O_3723
    • O_3724
    • O_3726
    • O_3727
    • O_3728
    • O_3729
    • H_1947
    • O_3720
    • O_3730
    • O_3725
    • O_4300
    • O_3732
    • H_772
    • O_3733
    • H_3735
    • O_3734
    • O_3739
    • H_3738
    • O_3740
    • O_3741
    • O_4301
    • O_2742
    • O_2803
    • O_3742
    • H_2452
    • H_2453
    • O_4302
    • O_2738
    • O_2739
    • O_2740
    • O_2741
    • O_4303
    • O_3743
    • O_3745
    • O_3641
    • O_3746
    • O_3645
    • O_3744
    • O_3643
    • O_4304
    • O_3747
    • O_3699
    • O_3752
    • H_599
    • O_3621
    • O_3751
    • O_2560
    • H_3439
    • O_4305
    • O_3755
    • O_3756
    • O_3757
    • O_3758
    • O_3759
    • H_2163
    • O_4306
    • O_1756
    • O_1757
    • O_4307
    • H_793
    • O_1759
    • H_790
    • H_1953
    • H_1952
    • O_3761
    • O_3763
    • O_876
    • O_3764
    • O_3765
    • O_3629
    • O_749
    • O_1772
    • H_1954
    • O_689
    • O_2378
    • O_3568
    • O_751
    • O_268
    • O_269
    • O_270
    • O_271
    • O_272
    • O_273
    • O_274
    • O_275
    • O_276
    • O_277
    • O_278
    • O_279
    • O_280
    • O_281
    • O_282
    • O_284
    • O_285
    • H_848
    • O_290
    • H_808
    • H_725
    • H_809
    • H_810
    • O_291
    • H_847
    • H_849
    • O_292
    • O_293
    • O_294
    • H_811
    • O_295
    • H_818
    • O_297
    • H_768
    • O_300
    • O_301
    • O_304
    • H_734
    • O_305
    • H_840
    • O_306
    • H_735
    • O_307
    • O_308
    • H_856
    • O_309
    • H_783
    • H_787
    • O_310
    • H_813
    • H_819
    • O_311
    • H_843
    • H_756
    • O_312
    • H_777
    • O_313
    • O_314
    • O_315
    • O_4236
    • O_316
    • O_317
    • O_319
    • O_321
    • O_322
    • O_324
    • O_326
    • O_328
    • O_330
    • H_845
    • O_334
    • O_4105
    • O_4107
    • O_4106
    • O_2437
    • O_335
    • O_336
    • O_342
    • H_732
    • O_4108
    • H_727
    • H_728
    • O_359
    • H_729
    • H_762
    • O_4109
    • H_730
    • H_807
    • O_4110
    • H_851
    • O_4111
    • O_4113
    • O_4112
    • H_739
    • H_731
    • O_4114
    • O_4115
    • H_733
    • O_4116
    • O_4117
    • O_366
    • O_367
    • O_368
    • O_369
    • O_371
    • O_376
    • O_377
    • H_842
    • O_370
    • H_782
    • O_3766
    • H_850
    • O_4120
    • O_4137
    • H_726
    • O_355
    • O_283
    • O_286
    • O_287
    • O_327
    • O_329
    • O_318
    • O_302
    • O_303
    • O_343
    • O_354
    • O_352
    • O_353
    • O_899
    • O_4138
    • O_4139
    • O_4140
    • O_4141
    • O_382
    • O_383
    • H_752
    • H_857
    • H_858
    • O_385
    • O_4234
    • O_3579
    • O_401
    • O_402
    • O_403
    • H_780
    • H_776
    • H_595
    • H_832
    • H_548
    • H_794
    • H_795
    • O_3767
    • O_404
    • O_405
    • H_769
    • O_406
    • O_407
    • H_859
    • H_846
    • O_408
    • H_741
    • H_796
    • O_409
    • H_797
    • O_410
    • H_798
    • O_411
    • O_412
    • H_836
    • H_852
    • H_837
    • H_838
    • O_3768
    • H_1955
    • H_875
    • H_1957
    • H_561
    • O_3769
    • H_802
    • H_803
    • H_804
    • O_3773
    • H_770
    • H_861
    • H_743
    • H_799
    • O_416
    • H_853
    • H_774
    • O_418
    • O_423
    • O_424
    • O_419
    • H_820
    • H_757
    • O_2810
    • H_872
    • H_805
    • H_873
    • O_871
    • O_236
    • H_384
    • H_812
    • H_814
    • H_815
    • H_816
    • H_817
    • H_870
    • O_421
    • O_4135
    • O_1261
    • H_800
    • H_801
    • H_781
    • H_1394
    • H_1382
    • H_1395
    • O_433
    • O_435
    • O_436
    • O_437
    • O_439
    • O_438
    • O_440
    • O_443
    • O_441
    • O_442
    • O_444
    • O_445
    • H_835
    • O_4136
    • O_434
    • O_4118
    • O_4128
    • O_4129
    • O_349
    • O_4130
    • O_4131
    • O_4132
    • O_4133
    • O_332
    • O_4134
    • O_4119
    • O_4121
    • O_323
    • O_325
    • O_320
    • H_860
    • O_4122
    • H_742
    • O_4123
    • H_740
    • H_806
    • H_821
    • O_4124
    • O_345
    • O_4125
    • O_347
    • O_4126
    • O_339
    • O_4127
    • O_341
    • O_446
    • O_447
    • O_448
    • O_4308
    • O_4310
    • O_4309
    • O_350
    • O_509
    • O_510
    • O_519
    • O_4311
    • O_520
    • O_4330
    • H_1958
    • O_3777
    • O_3781
    • O_113