Thermo Fisher Scientific Ion Selective Electrodes Fluoride User Manual

Page 20

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Instruction Manual

Fluoride Electrode

- 17 -

TROUBLESHOOTING HINTS

Symptom Possible Causes

Next Step

Out of Range defective meter

check meter with shorting strap

Reading

(see meter instruction manual)


defective electrode

check electrode operation


electrodes not plugged

unplug electrodes and reset

in properly


reference electrode

be sure reference electrode is

not filled

filled


air bubble on membrane

remove bubble by re-dipping

electrode


Noisy or Unstable

defective meter

check meter with shorting strap

Readings (readings
continuously or

air bubble on membrane

remove bubble by re-dipping

rapidly changing)

electrode


TISAB not used

use recommended TISAB


meter or stirrer

ground meter or stirrer

not grounded


defective electrode

replace electrode


electrode exposed

soak electrode in fluoride

to interference

standard with added TISAB



Drift (reading

samples and standards

allow solutions to come to room

slowly changing at different temperatures

temperature before measurement

in one direction)

electrode exposed to

check section entitled

complexing agents

Complexation


incorrect reference

use recommended

filling solution

filling solution


Low Slope or

standards contaminated

prepare fresh standards

No Slope

or incorrectly made


TISAB not used

use recommended TISAB


standard used as TISAB

use TISAB


electrode exposed

check section entitled

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