VICI D-4-I-SH14-R User Manual

Page 3

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Table of Contents

Introduction

Description and Operating Principles ............................................................ 1
Safety Notes and Information ........................................................................ 2
Components of the Detector System ............................................................. 3

System Requirements

Components not Included with the Detector System ..................................... 4
System Purity ................................................................................................ 4
Gas Specifications ......................................................................................... 5

Installation

General Precautions ...................................................................................... 6
Mounting the Detector on the GC .................................................................. 6
Gas Connections ........................................................................................... 7

Installing and Purging the Gas Regulator ............................................... 7
Installing and Purging the Helium Purifier .............................................. 8
Connecting the Discharge Gas to the Detector ....................................... 8

Pulser Module Installation .............................................................................. 9
Detector Electrical Connections .................................................................... 10
Initial Power-Up ............................................................................................. 10
Capillary Column Connection ........................................................................ 12
Packed Column Connection .......................................................................... 12
Testing for Leaks ........................................................................................... 13

Mode Selection and Setup

Helium Ionization Mode ................................................................................. 14
Selective Photoionization Mode .................................................................... 14

Troubleshooting ................................................................................................... 16

High Background Current .............................................................................. 16
Low Sensitivity ............................................................................................. 16
No Peaks ...................................................................................................... 16
High Noise Level ........................................................................................... 17
Performing a Hydrogen Leak Test .................................................................. 17

Warranty ............................................................................................................. 18

Detector Performance Log ................................................................................... 19

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