Labconco FreeZone Clear Stoppering Chambers User Manual
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Chapter 3: Getting Started
Product Service: Domestic 1-800-522-7658, International 816-333-8811
• Most common compounds used in freeze drying processes, if
allowed to enter the vacuum pump, will degrade the oil and
cause damage to the vacuum pump.
• Sugars and proteins typically will have minimal negative effect
on any of the materials of construction.
When using compounds in the Freeze Dryer that are hostile to the
materials of construction, it is imperative the equipment is
thoroughly cleaned after use.
• Rubber and plastic components that have been exposed to
damaging compounds should be removed and flushed with
water.
• The oil in the vacuum pump should be checked often. It must
be changed if it is cloudy, shows particles or is discolored. The
useful life of vacuum pump oil can be extended if the vacuum
pump is operated for an extended period of time after a freeze
dry run. This allows contaminants to be purged from the hot
oil. This must be done with the inlet to the pump blocked off
to prevent air from free flowing through the pump. This is
accomplished by closing all sample valves on a clean, dry
freeze dry system and turning on the vacuum pump. If the
pump is operated at an elevated vacuum level (> 10mBar), oil
may be expelled from the pump and damage could occur.
Another way to extend the life of the vacuum pump is to install an
optional secondary trap in the line between the Freeze Dry System
and the vacuum pump. Contact Labconco for ordering
information.
With prudent maintenance the FreeZone Freeze Dry System will
provide years of service. Warranty on the affected parts will be
voided if maintenance has been obviously neglected. If you have
questions about using specific compounds in the Freeze Dry
System, contact Labconco Technical Service at 1-800-821-5525 or
816-333-8811 or e-mail:
.