Document Outline

• Table of contents
• Table of figures
• 1 Introduction
  • 1.1 The Titrando system
  • 1.2 Instrument description
  • 1.3 Titration modes – Measuring modes – Dosing commands
  • 1.4 About the documentation
    • 1.4.1 Symbols and conventions
  • 1.5 Safety instructions
    • 1.5.1 General notes on safety
    • 1.5.2 Electrical safety
    • 1.5.3 Working with liquids
    • 1.5.4 Flammable solvents and chemicals
    • 1.5.5 Recycling and disposal
• 2 Overview of the instrument
• 3 Installation
  • 3.1 Setting up the instrument
    • 3.1.1 Packaging
    • 3.1.2 Checks
    • 3.1.3 Location
  • 3.2 Connecting a controller
    • 3.2.1 Operation
      • 3.2.1.1 Connecting a Touch Control
      • 3.2.1.2 Connecting a computer
  • 3.3 Connecting MSB devices
    • 3.3.1 Connecting a dosing device
    • 3.3.2 Connecting a stirrer or titration stand
    • 3.3.3 Connecting a Remote Box
  • 3.4 Connecting USB devices
    • 3.4.1 General
    • 3.4.2 Connecting a USB hub
    • 3.4.3 Connecting a printer
    • 3.4.4 Connecting a balance
    • 3.4.5 Connecting a PC keyboard (only for operation with Touch Control)
    • 3.4.6 Connecting a barcode reader
  • 3.5 Titration vessel for coulometric KF titration
    • 3.5.1 Mounting the coulometer cell
    • 3.5.2 Coulometer cell – Standard setup
    • 3.5.3 Coulometer cell with addition and aspiration tube (utilization with Ti Stand)
    • 3.5.4 Coulometer cell with aspiration equipment (utilization with Dosino)
    • 3.5.5 Coulometer cell with Karl Fischer oven
    • 3.5.6 Coulometer cell with sample changer
  • 3.6 Connecting sensors
    • 3.6.1 Connecting a generator electrode
    • 3.6.2 Connecting an indicator electrode
    • 3.6.3 Connecting a temperature sensor
• 4 Coulometric titration
  • 4.1 Principle of coulometry according to Karl Fischer
  • 4.2 Working with water standards
    • 4.2.1 Certified water standards
    • 4.2.2 Practical recommendations
  • 4.3 Sample addition
    • 4.3.1 Size of the sample size
    • 4.3.2 Working with liquid samples
    • 4.3.3 Working with solid samples
  • 4.4 Optimum working conditions
    • 4.4.1 General
    • 4.4.2 Drift
    • 4.4.3 Reagent replacement
    • 4.4.4 Indicator electrode
• 5 Operation and maintenance
  • 5.1 General notes
    • 5.1.1 Care
    • 5.1.2 Maintenance by Metrohm Service
  • 5.2 Generator electrode
    • 5.2.1 Generator electrode without diaphragm
      • 5.2.1.1 Reagents
      • 5.2.1.2 Cleaning
    • 5.2.2 Generator electrode with diaphragm
      • 5.2.2.1 Reagents
      • 5.2.2.2 Cleaning
  • 5.3 Quality Management and qualification with Metrohm
• 6 Troubleshooting
  • 6.1 General
  • 6.1 Karl Fischer titration
• 7 Appendix
  • 7.1 Remote interface
    • 7.1.1 Pin assignment of the remote interface
• 8 Technical specifications
  • 8.1 Measuring interface
    • 8.1.1 Generator electrode
    • 8.1.2 Indicator electrode
    • 8.1.3 Temperature
  • 8.2 Power connection
  • 8.3 Safety specifications
  • 8.4 Electromagnetic compatibility (EMC)
  • 8.5 Ambient temperature
  • 8.6 Interfaces
• 9 Warranty (guarantee)
• 10 Accessories
  • 10.1 Scope of delivery
    • 10.1.1 2.851.0010
    • 10.1.2 2.851.0020
    • 10.1.3 2.851.0110
    • 10.1.4 2.851.0120
  • 10.2 Optional accessories
• Index