Problem solving, Quick guide to problem solving – SSI America BINARY SOLVENT DELIVERY MODULE 90-2581 REV B User Manual

Page 36

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6. PROBLEM

SOLVING

Quick Guide to Problem Solving

You Notice

1. Uneven pressure

trace.

2. Pressure drops.
3. No flow out the

outlet check valve.

This May Mean

1. Bubble in

check valve.

2. Leaks in

system.

3. Dirty check

valve.

4. Bad check

valve.

Possible Cause

1. Solvent not properly

degassed.

2. Fittings are not tight.
3. Mobile phase not properly

filtered.

4. Particles from worn piston

seal caught in check valve.

5. Plugged inlet filter.

You Should

1. Check to be certain that mobile phase is

properly degassed.

2. Check connections for leaks by tightening

fittings.

3. Prime the system directly from the outlet

check valve.

4. Clean or replace the check valves. See

Section 5.4.

5. Clean or replace inlet filter. See Section

5.1.1.

1. Uneven pressure

trace.

2. Pressure drops.
3. Fluid between the

pump head and the
retainer.

1. Leaks in

system.

2. The piston

seal or
diaphragm is
worn.

1. Fittings not tight.
2. Long usage time since last

seal / diaphragm change.

3. Salt deposits on seal or

diaphragm (especially if
buffered aqueous mobile
phases are used).

1. Check all connections for leaks.
2. Replace piston seal & diaphragm. See

Sections 5.2 and 5.3.

3. Check the piston for salt deposits. Clean as

necessary. See Section 5.2.4.

Pump makes a loud
clanging or slapping
noise (intermittent
contact with cam).

Piston carrier is
catching in
piston guide.

1. Cap nut screws on the pump

head are loose.

2. Seal(s) are worn.
3. Piston guide is worn

1. Check cap nut screws on pump head.

Tighten if necessary.

2. Replace seals.
3. Replace piston guide and seals. See

Sections 5.2 and 5.3.

No power when pump
turned ON.

Blown fuses in
the power entry
module.

1. Power surge.
2. Internal short.

1. Replace only with the appropriate fuses (1A

for 100/110 Vac or 1/2A for 220/240 Vac).

2. Contact service technician if problem

persists.

Blue dye in mobile
phase.

Pulse damper
diaphragm has
burst.

Sudden pressure drop when
purging system.

Replace pulse damper. See Section 5.5.

Pump runs for 50
pump strokes, then
shuts down.

Lower pressure
limit is
activating.

1. Mobile phase is not properly

filtered.

2. Particles from worn seal

trapped in the system (e.g.,
tubing, filters, injection valve,
column inlet).

1. Check to be certain the low pressure limit is

set to 0 psi.

2. Only increase the low pressure limit after the

pump attains operating pressure.

3. Contact service technician.

1. Pump shuts down

after run is called
even with no
column connected.

2. Pump runs to

maximum pressure
and shuts down.

Clog in fluid
system.

1. Remove and clean both the inlet and

bulkhead filters. See Section 5.2.

2. If the problem persists, remove tubing from

system one piece at a time until you find the
clogged piece. Most clogs occur outside the
pump itself.

No power when pump
turned ON. Fan does
not run.

Blown fuses in
the power entry
module.

1. Power surge.
2. Internal short.

1. Replace only with the appropriate fuses (1A

for 100-120 Vac or 1/2A for 220-240 Vac).

2. Contact service technician if problem

persists.

Front panel appears
OK but pump motor
does not run.

Blown fuse on
the motor power
circuit board.

1. Power surge.
2. Internal short.

1. Replace only with the appropriate fuse .
2. Contact service technician if problem

persists.

PEEK fittings or
components leak.

You cannot
force PEEK
parts with
interference to
seal by brute
force tightening.

1. Film of fluid between

surfaces.

2. Salt crystals between

surfaces.

3. Scratches in mating surfaces.

1. Clean and dry mating surfaces.
2. If scratched, replace defective part.

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