Metrohm 907 Titrando User Manual

Page 6

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Table of contents

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IV

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907 Titrando

3.6.3

Connecting a polarizable electrode ........................................ 29

3.6.4

Connecting a temperature sensor or an electrode with inte-
grated temperature sensor ....................................................
30

3.6.5

Connecting an iConnect ........................................................ 30

3.6.6

Differential potentiometry ...................................................... 31

4 Karl Fischer titration

33

4.1

Volumetric titration ............................................................ 33

4.1.1

Principle of the volumetric Karl Fischer titration ...................... 33

4.1.2

Endpoint determination ......................................................... 33

4.1.3

Karl Fischer reagents .............................................................. 34

4.1.4

Application of the Karl Fischer titration .................................. 34

4.1.5

Working with water standards ............................................... 34

4.1.6

Sample addition .................................................................... 36

4.1.7

Optimum working conditions ................................................ 38

5 Operation and maintenance

40

5.1

General notes ...................................................................... 40

5.1.1

Care ...................................................................................... 40

5.1.2

Maintenance by Metrohm Service .......................................... 40

5.2

Quality management and qualification with Metrohm . . 41

6 Troubleshooting

42

6.1

General ................................................................................ 42

6.2

Karl Fischer titration .......................................................... 42

6.2.1

............................................................................................. 42

6.3

SET titration ........................................................................ 44

6.3.1

............................................................................................. 44

7 Appendix

45

7.1

Remote interface ................................................................ 45

7.1.1

Pin assignment of the remote interface .................................. 45

8 Technical specifications

49

8.1

Measuring interface ........................................................... 49

8.1.1

Potentiometry ........................................................................ 49

8.1.2

Temperature .......................................................................... 49

8.1.3

Polarizer ................................................................................ 50

8.2

Power connection ............................................................... 51

8.3

Safety specifications ........................................................... 51

8.4

Electromagnetic compatibility (EMC) ................................ 51

8.5

Ambient temperature ......................................................... 52

8.6

Reference conditions .......................................................... 52

8.7

Dimensions .......................................................................... 52

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