Metrohm 940 Professional IC Vario ONE/ChS User Manual

Page 6

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Table of contents

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IV

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940 Professional IC Vario ONE/ChS (2.940.1200)

3.13.2

Connecting the suppressor .................................................... 33

3.14 Installing the detector ........................................................ 38

3.15 Connecting the sample degasser (optional) ..................... 39

3.16 Connecting the instrument to a computer ....................... 41

3.17 Connecting the instrument to the power supply ............. 42

3.18 Initial start-up ..................................................................... 43

3.19 Connecting and rinsing the guard column ....................... 45

3.20 Connecting the separation column ................................... 47

3.21 Conditioning ........................................................................ 50

4 Operation

52

5 Operation and maintenance

53

5.1

IC system ............................................................................. 53

5.1.1

Operation .............................................................................. 53

5.1.2

Care ...................................................................................... 53

5.1.3

Maintenance by Metrohm Service .......................................... 53

5.1.4

Shutting down and starting back up ...................................... 54

5.2

Capillary connections ......................................................... 55

5.3

Servicing the door .............................................................. 55

5.4

Column thermostat – Replacing the capillaries ............... 55

5.5

Handling the eluent ............................................................ 57

5.5.1

Manufacturing eluent ............................................................ 57

5.5.2

Changing the eluent .............................................................. 58

5.6

Servicing the eluent degasser ........................................... 58

5.7

Notes on operating the high-pressure pump ................... 59

5.8

Servicing the high-pressure pump .................................... 60

5.9

Servicing the inline filter .................................................... 73

5.10 Servicing the pulsation absorber ...................................... 76

5.11 Injection valve ..................................................................... 76

5.12 Suppressor .......................................................................... 76
5.12.1

Notes for operating the suppressor ........................................ 76

5.12.2

Taking care of the suppressor housing ................................... 77

5.12.3

Servicing the suppressor ........................................................ 77

5.13 Servicing the detector ........................................................ 84

5.14 Rinsing the sample path .................................................... 84

5.15 Separation column ............................................................. 85
5.15.1

Separating efficiency .............................................................. 85

5.15.2

Protecting the separation column .......................................... 86

5.15.3

Storing the separation column ............................................... 86

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