2 tubing connections for sample flow path, Tubing connections for sample flow path – Metrohm 837 IC Degasser User Manual

Page 18

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2 Installation

837 IC (Eluent/Sample/Combi) Degasser/ Instructions for Use 8.837.1003

12

2.2.2

Tubing connections for sample flow path

To install the tubing connections for degassing of samples (with 837 IC

Sample Degasser or 837 IC Combi Degasser) proceed as follows:

1 Connect sample changer with degasser

To connect sample changer and degasser, a connection tubing

6.1834.050 is used. The tube end with the clamping screw is

connected via PEEK Coupling 6.2744.030 or 6.2744.034 to the

pump tubing of the peristaltic pump (see Instructions for Use of

the sample changer). Screw the other tube end with the pres-

sure screw and the flange to the Sample Inlet In (7) of the de-

gasser (Initially, screw it in loosely by hand, then tighten it by us-

ing the wrench ¼" 6.2621.050 (also included in the standard

equipment) to rotate the screw a further ¼ turn).

2 Connect degasser with injection valve

To connect degasser and injection valve, another connection

tubing 6.1834.050 is used. Screw the tube end with the pressure

screw and the flange to the corresponding Sample Outlet Out

(8) of the degasser (Initially, screw it in loosely by hand, then

tighten it by using the wrench ¼" 6.2621.050 (also included in

the standard equipment) to rotate the screw a further ¼ turn).

Screw the other end with the clamping screw to the injection

valve.

After installation is a good moment for the determination of the "Trans-

fer time" of the sample flow (The time the sample needs to flow from

the sample changer through the degasser till the end of the sample

loop), see section 4.4.1. The "Transfer time" is important to know for

the determination of the rinsing time – the longer the "Transfer time" is,

the longer the rinsing time should be.


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