Hach-Lange ISENa38103 User Manual

Page 13

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Message or symptom

Possible cause

Action

Slow stabilization time

Tape not removed from the filling hole

Remove the tape.

Contaminated glass sensor

Clean the probe (refer to

Clean the probe

on page 11).

Contaminated filling solution

Drain and replace the filling solution with fresh
solution.

Filling-hole cap is closed

Open the filling-hole cap while in use.

Low sample temperature or
temperature difference between
samples

Check the sample temperature. The lower the
temperature or the greater the difference of
temperatures between samples, the longer the
response time.

Air bubbles around inner reference
electrode

Gently tap the probe with hand or shake the
probe downward to remove any air bubbles.

Slope out of range (refer to

Check probe response

on page 14)

pH is too low

Make sure the pH is greater than 9 after each
ISA addition.

Ionic strength adjustor (ISA) not used

Add ISA to each sample and standard.

Insufficient conditioning

Condition for at least 8 hours in storage solution.

Damaged probe

Contact a Technical Support Representative.

Incorrect standards

Calibrate using freshly prepared standards.

Contaminated glass sensor

Clean the probe and recalibrate.

Air bubbles around inner reference
electrode

Gently tap the probe with hand or shake the
probe downward to remove any air bubbles.

Drifting/inaccurate readings

Contaminated glass bulb

Clean the probe (refer to

Clean the probe

on page 11).

Clogged reference

Rinse the reference junction with ISA rinse
solution thoroughly and shake the probe
downward to remove any air bubbles.

Improper storage
conditions/dehydrated glass bulb

Clean or condition the probe and attempt another
calibration. The probe may not function correctly
if the probe has been left dry for extended
periods of time. To re-condition the glass sensor
and reference junctions, allow the probe to soak
in storage solution (that contains Sodium ISA) for
at least 8 hours before use.

Stabilization criteria not optimized for
the application

Adjust the stabilization criteria in the
Measurement Options menu.

Magnetic stirrers may generate
sufficient heat to change solution
temperature.

Put a piece of insulating material between the
stirrer and beaker.

Filling-hole cap is closed

Open the filling-hole cap while in use.

Damaged probe

Contact a Technical Support Representative.

Electromagnetic Forces (EMF) such as
voltaic cells, thermoelectric devices,
electrical generators, resistors and
transformers

Do not use in areas where EMF is present.

Colloidal and/or particulates in the
filling solution

Replace the filling solution, calibrate and retest.

Air bubbles around inner reference
electrode

Gently tap the probe with hand or shake the
probe downward to remove any air bubbles.

13

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