High noise level, Performing a hydrogen leak test – VICI D-3-I-7890 User Manual

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19

High Noise Level

If the noise lievel is high:

1. See if it improves with the GC fan turned off.

2. Check the column insertion position (10.3 cm for capillary columns,

8.7 cm for packed columns.)

3. If the noise level is still high, do a hydrogen leak test, described below.

4. If there are no leaks found, or leaks are found and repaired and the noise

level is still high, consult Valco.

Performing a Hydrogen Leak Test

A hydrogen leak test allows you to pinpoint loose fittings and leaks inside
the detector.

1. Connect a length of plastic tubing to a regulated hydrogen bottle.

Establish a flow of 5-10 ml/min.

2. Hold the hydrogen outlet tube at a fitting connection for ten seconds while

monitoring the baseline.

3. Tighten the fitting and test it again, repeating as necessary until every

connection has passed the ten second test.

4. Hold the hydrogen outlet close to the detector.

(Do not insert the tube into

any detector holes.) If a leak in the detector is indicated, contact Valco.

Troubleshooting

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