Metrohm 940 Professional IC Vario ONE/SeS/PP/Prep 2 User Manual

Page 6

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Table of contents

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IV

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940 Professional IC Vario ONE/SeS/PP/Prep 2 (2.940.1520)

3.13.2

Connecting the suppressor .................................................... 34

3.14 Peristaltic pump .................................................................. 38
3.14.1

Installing the peristaltic pump ................................................ 38

3.14.2

Mode of operation for the peristaltic pump ........................... 44

3.15 Metrohm CO

2

Suppressor (MCS) ....................................... 45

3.15.1

General information on MCS ................................................. 45

3.15.2

Connecting the MCS ............................................................. 46

3.15.3

Installing adsorption cartridges .............................................. 47

3.16 Installing the detector ........................................................ 49

3.17 Connecting the sample degasser (optional) ..................... 49

3.18 Installing the 6-port valve .................................................. 51

3.19 Connecting the instrument to a computer ....................... 52

3.20 Connecting the instrument to the power supply ............. 53

3.21 Initial start-up ..................................................................... 54

3.22 Connecting and rinsing the guard column ....................... 56

3.23 Connecting the separation column ................................... 58

3.24 Conditioning ........................................................................ 62

4 Operation

64

5 Operation and maintenance

65

5.1

IC system ............................................................................. 65

5.1.1

Operation .............................................................................. 65

5.1.2

Care ...................................................................................... 65

5.1.3

Maintenance by Metrohm Service .......................................... 65

5.1.4

Shutting down and starting back up ...................................... 66

5.2

Capillary connections ......................................................... 67

5.3

Servicing the door .............................................................. 67

5.4

Column thermostat – Replacing the capillaries ............... 67

5.5

Handling the eluent ............................................................ 69

5.5.1

Manufacturing eluent ............................................................ 69

5.5.2

Changing the eluent .............................................................. 70

5.6

Servicing the eluent degasser ........................................... 70

5.7

Notes on operating the high-pressure pump ................... 71

5.8

Servicing the high-pressure pump .................................... 72

5.9

Servicing the inline filter .................................................... 85

5.10 Servicing the pulsation absorber ...................................... 88

5.11 Injection valve ..................................................................... 88

5.12 Suppressor .......................................................................... 88
5.12.1

Notes for operating the suppressor ........................................ 88

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