Metrohm 940 Professional IC Vario ONE/ChS/LPG User Manual

Page 6

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Table of contents

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IV

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940 Professional IC Vario ONE/ChS/LPG (2.940.1250)

3.13.2

Connecting the suppressor .................................................... 33

3.14 Installing the detector ........................................................ 38

3.15 Connecting the sample degasser (optional) ..................... 39

3.16 Low-pressure gradient ....................................................... 41

3.17 Installing the low-pressure gradient ................................. 43

3.18 Connecting the instrument to a computer ....................... 44

3.19 Connecting the instrument to the power supply ............. 45

3.20 Initial start-up ..................................................................... 46

3.21 Connecting and rinsing the guard column ....................... 49

3.22 Connecting the separation column ................................... 51

3.23 Conditioning ........................................................................ 54

4 Operation

56

5 Operation and maintenance

57

5.1

IC system ............................................................................. 57

5.1.1

Operation .............................................................................. 57

5.1.2

Care ...................................................................................... 57

5.1.3

Maintenance by Metrohm Service .......................................... 57

5.1.4

Shutting down and starting back up ...................................... 58

5.2

Capillary connections ......................................................... 59

5.3

Servicing the door .............................................................. 59

5.4

Column thermostat – Replacing the capillaries ............... 59

5.5

Handling the eluent ............................................................ 61

5.5.1

Manufacturing eluent ............................................................ 61

5.5.2

Changing the eluent .............................................................. 62

5.6

Servicing the eluent degasser ........................................... 62

5.7

Notes on operating the high-pressure pump ................... 63

5.8

Servicing the high-pressure pump .................................... 64

5.9

Servicing the inline filter .................................................... 77

5.10 Servicing the pulsation absorber ...................................... 80

5.11 Injection valve ..................................................................... 80

5.12 Suppressor .......................................................................... 80
5.12.1

Notes for operating the suppressor ........................................ 80

5.12.2

Taking care of the suppressor housing ................................... 81

5.12.3

Servicing the suppressor ........................................................ 81

5.13 Servicing the detector ........................................................ 88

5.14 Rinsing the sample path .................................................... 88

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