Metrohm 915 KF Ti-Touch User Manual

915 kf ti-touch

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915 KF Ti-Touch

Manual

8.915.8005EN / 2014-03-10

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Table of contents

Document Outline

Table of contents
Table of figures
1 Introduction
- 1.1 Instrument description
- 1.2 About the documentation
  - 1.2.1 Symbols and conventions
2 Safety instructions
- 2.1 General notes on safety
- 2.2 Electrical safety
- 2.3 Tubing and capillary connections
- 2.4 Flammable solvents and chemicals
- 2.5 Recycling and disposal
3 Overview of the instrument
- 3.1 Front of the instrument
- 3.2 Rear of the instrument
4 Installation
- 4.1 Setting up the instrument
- 4.2 Connecting the power supply unit
- 4.3 Connecting MSB devices
- 4.4 Connecting USB devices
- 4.5 Setting up the titration vessel
- 4.6 Connecting sensors
- 4.7 Connecting the Ti-Touch to a network
5 Titrations
- 5.1 Water determination according to Karl Fischer (KFT)
6 Operation
- 6.1 Switching the instrument on and off
- 6.2 Fundamentals of operation
7 System settings
- 7.1 General system settings
  - 7.1.1 Selecting the dialog language
  - 7.1.2 Setting the date, time and local time
- 7.2 System-specific dialog options
- 7.3 User administration
- 7.4 Measured value display
- 7.5 Acoustic signals
8 Titrants
- 8.1 Adding a new titrant
- 8.2 Editing titrant data
- 8.3 Monitoring the working life
- 8.4 Dosing unit
- 8.5 Exchange unit
  - 8.5.1 Parameters for the preparation (PREP)
  - 8.5.2 Tubing parameters
- 8.6 GLP test for exchange unit and dosing unit
- 8.7 Titer determination options and data
  - 8.7.1 Titer validity
  - 8.7.2 Properties of the previous titer determinations
9 Reagents
- 9.1 Editing reagent data
- 9.2 Reagent monitoring
10 Sensors
- 10.1 Adding a new sensor
- 10.2 Editing the sensor data
- 10.3 Monitoring the working life
11 Device manager
- 11.1 Adding a new device
- 11.2 Configuring the instrument
- 11.3 Ti‑Touch
- 11.4 Metrohm control devices
- 11.5 USB Sample Processor
- 11.6 Sample racks
  - 11.6.1 Editing rack data
  - 11.6.2 Rack adjustment
- 11.7 Printer
- 11.8 Balance
- 11.9 USB/RS-232 adapter
- 11.10 PC keyboard
- 11.11 Barcode reader
12 File manager
- 12.1 Managing files
- 12.2 External storage medium
- 12.3 Creating backups / Restoring data
  - 12.3.1 Restoring data
13 GLP manager
- 13.1 Automatic system test
- 13.2 Test tools
- 13.3 GLP tests for measurement and titration
  - 13.3.1 Parameter description
- 13.4 System validation
  - 13.4.1 Parameter description
- 13.5 System monitoring
  - 13.5.1 Service interval
  - 13.5.2 Backup interval
14 Common variables
- 14.1 Editing common variables
- 14.2 Properties of common variables
- 14.3 Monitoring validity
- 14.4 Assigning a result automatically to a common variable
15 Templates
- 15.1 Sample data
  - 15.1.1 Sample identification list
  - 15.1.2 Sample assignment table
- 15.2 Custom result templates
  - 15.2.1 Editing result templates
- 15.3 Input lines
  - 15.3.1 Editing the input signal
- 15.4 Output lines
  - 15.4.1 Editing the output signal
- 15.5 Report header
16 Methods
- 16.1 Creating a new method
- 16.2 Saving a method
- 16.3 Loading a method
- 16.4 Editing a method
  - 16.4.1 Inserting a command
- 16.5 Method options
17 Control
18 Favorites
- 18.1 Creating favorites
  - 18.1.1 Editing favorites
19 Sample data
- 19.1 Entering sample data in the main dialog
- 19.2 Requesting sample data at the start of the determination
20 Sample table
- 20.1 General
- 20.2 Edit the sample data
- 20.3 Properties
21 Determination run
- 21.1 Carrying out a single determination
- 21.2 Performing a sample series
- 21.3 Canceling determinations manually
22 Live modifications
- 22.1 Editing the sample data of the running determination
- 22.2 Editing the sample table while a determination is running
- 22.3 Live display
- 22.4 Live parameters
23 Results and more determination data
- 23.1 More determination data
  - 23.1.1 Details
- 23.2 Messages
- 23.3 Local common variables
- 23.4 Determination properties
- 23.5 Loading a determination
  - 23.5.1 Determination list
- 23.6 Saving a determination
- 23.7 Curves
- 23.8 Recalculation and reevaluation
24 Statistics
- 24.1 Displaying details for a result
- 24.2 Deleting statistical data
- 24.3 Adding a determination to a determination series
25 Result table
- 25.1 Properties
- 25.2 Saving the result table
- 25.3 Loading the result table
26 Printing
- 26.1 General report options
- 26.2 Settings of the individual reports
- 26.3 List of all printable reports
27 Manual control
- 27.1 Opening and closing the manual control
- 27.2 Measuring
  - 27.2.1 Parameter description
- 27.3 Dosing
- 27.4 Stirring
- 27.5 Remote
- 27.6 USB Sample Processor
28 Parameters
- 28.1 Volumetric Karl Fischer titrations (KFT)
- 28.2 Measurements (MEAS)
- 28.3 Evaluations (EVAL)
- 28.4 Calculations
- 28.5 Reports (REPORT)
- 28.6 Dosing and Liquid Handling
- 28.7 Communication
- 28.8 Automation
- 28.9 Miscellaneous commands
29 Operation and maintenance
- 29.1 System initialization
- 29.2 Quality management and qualification with Metrohm
30 Troubleshooting
- 30.1 Editing methods
- 30.2 Sample table
- 30.3 Results/Statistics
- 30.4 Printing
- 30.5 Manual control
- 30.6 Titration stand with pump
- 30.7 Karl Fischer titration
31 Appendix
- 31.1 Dosing unit
  - 31.1.1 Maximum dosing and filling rate
  - 31.1.2 Default parameters for preparing (PREP) and emptying (EMPTY)
- 31.2 Exchange unit
  - 31.2.1 Maximum dosing and filling rate
  - 31.2.2 Default parameters for preparing (PREP)
- 31.3 Stirring rate
- 31.4 Balance
- 31.5 Remote interface
  - 31.5.1 Pin assignment of the remote interface
- 31.6 Result variables as parameter setting
- 31.7 Diagnosis
- 31.8 Arithmetic algorithms in the Ti‑Touch
32 Technical specifications
- 32.1 Touch screen
- 32.2 Measuring inputs
  - 32.2.1 Polarizer
  - 32.2.2 Temperature
- 32.3 Internal stirrer
- 32.4 Pump
- 32.5 Interfaces
- 32.6 Power supply
- 32.7 Safety specifications
- 32.8 Electromagnetic compatibility (EMC)
- 32.9 Ambient temperature
- 32.10 Reference conditions
- 32.11 Dimensions
33 Warranty (guarantee)
34 Accessories
Index

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