Metrohm 850 Professional IC Anion MSM-HC MCS LP-Gradient User Manual

Page 6

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Table of contents

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IV

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850 Professional IC–Anion – MSM-HC – MCS – LP Gradient

3.12 High pressure pump ........................................................... 42
3.12.1

Capillary connections high pressure pump/purge valve ........... 42

3.12.2

Connecting low pressure gradient ......................................... 43

3.12.3

Deaerating the high pressure pump ....................................... 44

3.13 Inline filter ........................................................................... 46

3.14 Pulsation damper ............................................................... 47

3.15 Sample degasser ................................................................. 48

3.16 Injection valve ..................................................................... 50
3.16.1

Connecting the injection valve ............................................... 50

3.16.2

Mode of operation of the injection valve ............................... 51

3.16.3

Selecting the sample loop ...................................................... 52

3.17 Column thermostat ............................................................ 52

3.18 High Capacity Metrohm Suppressor Module

(MSM-HC) ............................................................................ 55

3.18.1

General information on the MSM-HC .................................... 55

3.18.2

Connecting the MSM-HC ....................................................... 55

3.19 Peristaltic pump .................................................................. 58
3.19.1

Principle of the peristaltic pump ............................................. 58

3.19.2

Installing the peristaltic pump ................................................ 59

3.20 Metrohm CO

2

suppressor (MCS) ....................................... 63

3.20.1

General information on the MCS ........................................... 63

3.20.2

Connecting MCS ................................................................... 63

3.20.3

Installing the adsorption cartridges ........................................ 64

3.21 Conductivity detector ......................................................... 66

3.22 Connecting the instrument ................................................ 69
3.22.1

Connecting the instrument to the PC ..................................... 69

3.22.2

Connecting the instrument to mains supply ........................... 69

3.23 Guard column ..................................................................... 70

3.24 Separation column ............................................................. 72

4 Start-up

74

4.1

Initial start-up ..................................................................... 74

4.2

Conditioning ........................................................................ 75

5 Operation and maintenance

77

5.1

General information ........................................................... 77

5.1.1

Care ...................................................................................... 77

5.1.2

Maintenance by Metrohm Service .......................................... 77

5.1.3

Operation .............................................................................. 78

5.1.4

Shutting down ...................................................................... 78

5.2

Capillary connections ......................................................... 78

5.2.1

Operation .............................................................................. 78

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