4 connections at injection valve, 1 general information, 2 attaching standard accessories – Metrohm 812 Valve Unit User Manual

Page 13: Fill, Inject

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2 Installation

812 Valve Unit

10

2.4

Connections at injection valve

2.4.1 General

information

The two six-way valves at the 812 Valve Unit each have 6 connections

for capillaries which are switched as follows:

Fill

1

2

3

6

4

5

Inject

1

2

3

6

4

5

Fig. 4: Switching of injection valves

Connections 1 and 2 of the valve are normally used for supply of sam-

ple solution, connections 4 and 5 for eluent supply, and connections 3

and 6 for sample loop installation. For solution supply in the low pres-

sure range (sample feed by use of a syringe or a peristaltic pump), the

6.1803.020 PTFE capillary (i.d. 0.97 mm) is used; in the high pressure

range, the 6.1831.010 PEEK capillary (i.d. 0.25 mm) is used. For both

capillaries, a 6.2744.010 PEEK compression fitting is used as connec-

tor.


2.4.2 Attaching

standard accessories

The standard accessories supplied with the 812 Valve Unit can be used

to equip one valve for manual filling of the sample loop. Proceed as fol-

lows (see Fig. 5):

1 Connecting the syringe

Cut off a piece of the 6.1803.020 PTFE capillary to the de-

sired length (at best using the optionally available 6.2621.080

tubing cutter) and fit it on both sides with a 6.2744.010 PEEK

compression fitting (do not tighten too firmly).

Screw one end of the PTFE capillary 13 to connection 1 of

the injection valve.

Screw the other end of the PTFE capillary 13 to the

6.2744.120 coupling.

Push 6.2816.020 syringe (without needle) as far as it will go

into the connection of the 6.2744.120 coupling.

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