Metrohm 930 Compact IC Flex Oven/SeS/Deg User Manual

Page 6

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Table of contents

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IV

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930 Compact IC Flex Oven/SeS/Deg (2.930.2460)

3.13 Metrohm CO

2

Suppressor (MCS) ....................................... 36

3.13.1

General information on MCS ................................................. 36

3.13.2

Connecting the MCS ............................................................. 37

3.13.3

Installing adsorption cartridges .............................................. 38

3.14 Installing the detector ........................................................ 40

3.15 Connecting the sample degasser (optional) ..................... 40

3.16 Connecting the instrument to a computer ....................... 42

3.17 Connecting the instrument to the power supply ............. 43

3.18 Initial start-up ..................................................................... 44

3.19 Connecting and rinsing the guard column ....................... 46

3.20 Connecting the separation column ................................... 48

3.21 Conditioning ........................................................................ 51

4 Operation

53

5 Operation and maintenance

54

5.1

IC system ............................................................................. 54

5.1.1

Operation .............................................................................. 54

5.1.2

Care ...................................................................................... 54

5.1.3

Maintenance by Metrohm Service .......................................... 54

5.1.4

Shutting down and starting back up ...................................... 55

5.2

Capillary connections ......................................................... 56

5.3

Servicing the door .............................................................. 56

5.4

Column oven – replacing the capillaries ........................... 56

5.5

Handling the eluent ............................................................ 58

5.5.1

Manufacturing eluent ............................................................ 58

5.5.2

Changing the eluent .............................................................. 59

5.6

Servicing the eluent degasser ........................................... 59

5.7

Notes on operating the high-pressure pump ................... 60

5.8

Servicing the high-pressure pump .................................... 61

5.9

Servicing the inline filter .................................................... 74

5.10 Servicing the pulsation absorber ...................................... 77

5.11 Injection valve ..................................................................... 77

5.12 Suppressor .......................................................................... 77
5.12.1

Notes for operating the suppressor ........................................ 77

5.12.2

Taking care of the suppressor housing ................................... 78

5.12.3

Servicing the suppressor ........................................................ 78

5.13 Servicing the Metrohm CO

2

Suppressor (MCS) ................ 85

5.13.1

Replacing the CO

2

adsorption cartridge ................................. 85

5.13.2

Regenerating the H

2

O adsorption cartridge ............................ 85

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