Metrohm 850 Professiona IC Cation Prep 1 User Manual

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Table of contents

850 Professional IC –Cation – Prep 1

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III

Table of contents

1 Introduction

1

1.1

Instrument description ......................................................... 1

1.2

Intended use ......................................................................... 4

1.3

About the documentation ................................................... 5

1.3.1

Symbols and conventions ........................................................ 5

1.4

Safety instructions ................................................................ 6

1.4.1

General notes on safety ........................................................... 6

1.4.2

Electrical safety ........................................................................ 6

1.4.3

Tubing and capillary connections ............................................. 7

1.4.4

Flammable solvents and chemicals ........................................... 7

1.4.5

Recycling and disposal ............................................................. 7

2 Installation

9

2.1

About this chapter ................................................................ 9

2.2

Initial installation .................................................................. 9

2.3

Flow diagram ...................................................................... 10

2.4

Setting up the instrument .................................................. 15

2.4.1

Packaging .............................................................................. 15

2.4.2

Checks .................................................................................. 15

2.4.3

Location ................................................................................ 15

2.5

Capillary connections in the IC system ............................. 16

2.6

Rear of the instrument ....................................................... 18

2.6.1

Rollers and handle ................................................................. 18

2.6.2

Positioning and connecting the detector ................................ 21

2.6.3

Transport locking screws ....................................................... 23

2.6.4

Leak sensor ........................................................................... 23

2.6.5

Drainage tubing ..................................................................... 24

2.7

Capillary and cable feed-throughs .................................... 26

2.8

Eluent ................................................................................... 29

2.8.1

Connecting eluent bottle ....................................................... 29

2.9

Eluent degasser ................................................................. 33

2.10 High pressure pump ........................................................... 34
2.10.1

Capillary connections high pressure pump/purge valve ........... 34

2.10.2

Deaerating the high pressure pump ....................................... 37

2.11 Inline filter ........................................................................... 39

2.12 Pulsation damper ............................................................... 40

2.13 Sample degasser ................................................................. 42

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