BUCHI Melting Point M-560 - Manual (Page 30)

6 Operation
30 Melting Point M-560 Operation Manual, Version D
• Delay: to ensure equilibrium
between oven temperature
and sample temperature.
During this delay time some
air bubbles escape from the
boiling point capillary. This
request can be changed in
the setting “Boiling sample
conditioning” (see 6.5). Bubble
frequency is an indicator.
When frequency of air bubbles
coming out of the capillary is
equal the indicator press
Set.
• To run through the result,
turn the rotary knob up and
down.
• Press End or STOP to
return to the idle screen.
• Press START to measure
again with the identical
measuring parameters.
6.3.3 Creating a method
NOTE
The process of creating a boiling point method is identical that used to create a melting point method
(see 6.2.3).
6.3.4 Adjusting parameters during a determination
During preheating or a determination, measuring parameters can be modified. This function is possible
only if enabled by the setting “Param. adj. during meas.” (see 6.5).
a
• Turning the rotary knob
displays the current param-
eter set.
• Adjust the parameters by
pressing Edit. Adjusting the
parameters does not affect
the saved method.
• If the temperature gradient
is changed during a measure-
ment, the result shows
CHANGED (a) for the
temperature gradient.