In-Situ TROLL 9500 Operators Manual User Manual

Page 117

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112

TROLL 9500 Operator’s Manual

0095110 rev. 007 01/09

CHLORIDE CALIBRATION PROCEDURE

1. Rinse the Cal Cup and front end of the MP TROLL 9500 in clean

water. Rinse very thoroughly if the chloride sensor has recently
been exposed to pH buffers during a pH calibration. Shake to dry.

For best results, follow this with a rinse in a portion of the selected

calibration solution. Discard the rinse solution.

2. Insure the black PVC base (or the stirrer) is attached to the Cal

Cup, and fill the Cal Cup to the fill line with the selected calibration
solution.

s

point calibration.

s

use the lower line as a guide.

s

to the upper line.

3. Insert the front end of the MP TROLL 9500

into the open end of the Cal Cup. Thread the
Cal Cup onto the body until seated against the
o-ring, then back off slightly to avoid overtight-
ening.

To stabilize the instrument, you may wish to

use a calibration stand or other support.

4. Connect the MP TROLL 9500 to a PC and

establish a connection in Win-Situ 4 or Pocket-
Situ 4. Win-Situ screens are illustrated here.
The Pocket-Situ interface is similar, with the
Navigation tree at the top of the screen and
the Information pane below it.

5. Select the MP TROLL 9500 in the Navigation

tree.

The software will automatically detect and display the installed sen-

sors. If one or more sensors is installed in the wrong port, an error
message will be displayed. Simply remove the sensor and install it
in the correct position, then “refresh” the device before continuing.

6. Select Chloride in the Parameters list. The sensor serial number

(S/N) and recent calibration information is displayed.

7. Select Calibrate.

The Chloride Calibration Wizard starts. A screen like this is dis-

played.

8. Select the number of calibration points for this calibration, and the

concentration (ppm) of the calibration solution for each point.

Cal point 1 is the solution the sensor is soaking in now, the lowest

concentration for a multi-point calibration. If doing a three-point
bithermal cal, choose cal point 3 to be the same as either cal point
1 or cal point 2.

9. Select Next to continue.

6

7

8

9

SECTION 16: CHLORIDE

3

Cal Cup

Stirrer

(optional)

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