Inhalt – Metrohm NIRS XDS RapidContent Analyzer User Manual

Page 5

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Inhalt

1

Introduction to XDS™ Rapid Content Analyzer .............................................................. 5

2

Site Readiness ................................................................................................................ 8

2.1

Temperature and Humidity ........................................................................... 8

2.2

General Environment .................................................................................... 8

2.3

Vibration ....................................................................................................... 8

2.4

Electrical Power ............................................................................................ 8

2.5

Instrument Communication .......................................................................... 8

2.6

Instrument Dimensions and Weight .............................................................. 9

3

XDS Instrument Connection ......................................................................................... 10

3.1

Network Connection ................................................................................... 10

3.2

Direct Connection ....................................................................................... 11

3.3

Overview of XDS Instrument Communication ............................................. 11

3.4

Flowchart Diagram of XDS communication protocol .................................. 12

3.4.1

Microsoft Windows Firewalls ................................................................................ 13

3.4.2

Network Evolution Issues ...................................................................................... 13

3.4.3

Quick Glossary of Terms: ....................................................................................... 13

3.5

Connection in Vision ................................................................................... 14

3.6

Troubleshooting Connection Problems ....................................................... 15

3.6.1

Network Troubleshooting Overview ...................................................................... 16

3.6.2

Direct Connection Troubleshooting Overview ........................................................ 19

4

Assembly of the Instrument ......................................................................................... 21

5

Rapid Content Module ................................................................................................. 26

5.1

Sample Cell ................................................................................................. 26

5.1.1

Loading the sample cell: ....................................................................................... 27

5.2

Use of the Sample Transport Mechanism .................................................... 29

Removal of Sample Carriage: ....................................................................................... 30

Installation of Iris Adapter:........................................................................................... 31

5.3

Spot Size Adjustment .................................................................................. 32

6

Vision Software: Connection to the Instrument ............................................................ 35

7

Instrument Diagnostics................................................................................................. 39

7.1

Setup Diagnostics ....................................................................................... 39

7.1.1

Wavelength Linearization ...................................................................................... 40

7.1.2

Reference Standardization .................................................................................... 41

7.1.3

Instrument Calibration .......................................................................................... 46

Information about the wavelength standard: ............................................................... 48

7.1.4

IPV Setup (Instrument Performance Verification) ................................................... 49

7.2

Evaluation Diagnostics ................................................................................ 51

7.2.1

Performance Test .................................................................................................. 51

7.2.2

Wavelength Certification ...................................................................................... 53

7.2.3

Photometric Test .................................................................................................. 57

7.2.4

Gain Test .............................................................................................................. 60

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