10 servicing the pulsation absorber, 11 injection valve, 12 servicing the detector – Metrohm 940 Professional IC Vario ONE/Proep 2 User Manual

Page 82: 13 rinsing the sample path

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5.10 Servicing the pulsation absorber

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940 Professional IC Vario ONE/Prep 2 (2.940.1120)

5.10

Servicing the pulsation absorber

CAUTION

The pulsation absorber is maintenance-free and must not be opened.

5.11

Injection valve

Maintenance on the injection valve is best performed by specialist person-
nel from Metrohm during annual service.

5.12

Servicing the detector

Follow the maintenance instructions in the the detector's manual.

5.13

Rinsing the sample path

Before a new sample is measured, the sample path has to be rinsed with it
long enough to prevent the measuring result from being falsified by the
previous sample (sample carry-over).

The time required to rinse the sample path with the new sample is called
the rinsing time. The rinsing time depends on the transfer time.

The transfer time corresponds to the time the sample needs to flow from
the sample vessel to the end of the sample loop. The transfer time
depends on the following factors:

The pump capacity of the peristaltic pump or Dosino

The total capillary volume

The volume of the gas removed from the sample by the sample degas-
ser

The transfer time can be determined as follows:

Determining the transfer time

1 Emptying the sample path

Pump air through the sample path (pump tubing, tubing connec-
tions, capillary in the degasser, sample loop) for several minutes until
all liquid is displaced by the air.

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