Metrohm 930 Compact IC Flex SeS User Manual

Page 6

Advertising
background image

Table of contents

■■■■■■■■■■■■■■■■■■■■■■

IV

■■■■■■■■

930 Compact IC Flex SeS (2.930.1400)

3.11.3

Installing adsorption cartridges .............................................. 38

3.12 Installing the detector ........................................................ 40

3.13 Connecting the instrument to a computer ....................... 40

3.14 Connecting the instrument to the power supply ............. 41

3.15 Initial start-up ..................................................................... 42

3.16 Connecting and rinsing the guard column ....................... 45

3.17 Connecting the separation column ................................... 47

3.18 Conditioning ........................................................................ 50

4 Operation

52

5 Operation and maintenance

53

5.1

IC system ............................................................................. 53

5.1.1

Operation .............................................................................. 53

5.1.2

Care ...................................................................................... 53

5.1.3

Maintenance by Metrohm Service .......................................... 53

5.1.4

Shutting down and starting back up ...................................... 54

5.2

Capillary connections ......................................................... 55

5.3

Servicing the door .............................................................. 55

5.4

Handling the eluent ............................................................ 55

5.4.1

Manufacturing eluent ............................................................ 56

5.4.2

Changing the eluent .............................................................. 56

5.5

Notes on operating the high-pressure pump ................... 57

5.6

Servicing the high-pressure pump .................................... 58

5.7

Servicing the inline filter .................................................... 71

5.8

Servicing the pulsation absorber ...................................... 74

5.9

Injection valve ..................................................................... 74

5.10 Suppressor .......................................................................... 74
5.10.1

Notes for operating the suppressor ........................................ 74

5.10.2

Taking care of the suppressor housing ................................... 75

5.10.3

Servicing the suppressor ........................................................ 75

5.11 Servicing the Metrohm CO

2

Suppressor (MCS) ................ 82

5.11.1

Replacing the CO

2

adsorption cartridge ................................. 82

5.11.2

Regenerating the H

2

O adsorption cartridge ............................ 82

5.12 Servicing the detector ........................................................ 83

5.13 Rinsing the sample path .................................................... 83

5.14 Separation column ............................................................. 84
5.14.1

Separating efficiency .............................................................. 84

5.14.2

Protecting the separation column .......................................... 85

5.14.3

Storing the separation column ............................................... 85

5.14.4

Regenerating the separation column ...................................... 85

Advertising