Table of contents
EN
1
About this Document .................................................................................................... 1
1.1
Versions references ........................................................................................................................... 1
1.2
About this manual .............................................................................................................................. 1
1.2.1
Reference documents ...................................................................................................................... 1
1.2.2
Icons and symbols ........................................................................................................................... 2
2
Basic safety instructions .............................................................................................. 5
2.1
General Safety Instructions .............................................................................................................. 5
2.2
Intended use ....................................................................................................................................... 5
2.3
Improper Use ...................................................................................................................................... 5
2.4
Use in explosion-prone areas ........................................................................................................... 6
2.5
Responsibilities of the operator ....................................................................................................... 6
2.6
Responsibilities of the operating personnel ................................................................................... 6
2.7
Qualifications of Personnel ............................................................................................................... 7
2.8
Safety Conscious Working ................................................................................................................ 7
2.9
Safety devices on the equipment ..................................................................................................... 7
2.10
Signs on the equipment .................................................................................................................... 8
2.11
Remaining hazards ............................................................................................................................ 8
3
Unit Description ...........................................................................................................11
4
Set-up and Start-up ......................................................................................................12
4.1
Scope of delivery ............................................................................................................................. 12
4.2
Transport .......................................................................................................................................... 14
4.2.1
Removing the transportation safety device .................................................................................... 14
4.2.2
Attaching the transportation protection device before packing ...................................................... 14
4.3
Setting up the basic unit ................................................................................................................. 15
4.4
Start-up ............................................................................................................................................. 15
4.4.1
Installing the heating bath .............................................................................................................. 15
4.4.2
Fill the heating bath ....................................................................................................................... 16
4.4.3
Offsetting the heating bath ............................................................................................................. 16
4.4.4
Heating bath set-up when using Rotacool ..................................................................................... 16
4.4.5
Connect the base unit .................................................................................................................... 17
4.4.6
Operating the lift ............................................................................................................................ 19
4.5
Assemble glassware sets ................................................................................................................ 19
4.5.1
Install the condenser mounting (G3-G6) ........................................................................................ 20
4.5.2
Install the vapor tube ..................................................................................................................... 21
4.5.3
Install the condenser ...................................................................................................................... 23
4.5.4
Mount the vertical condenser (G3-G6) in the condenser bracket................................................... 25
4.5.5
Install the evaporator flask ............................................................................................................. 26
4.5.6
Setting the evaporator flask inclination .......................................................................................... 27
4.5.7
Setting the immersion depth of the evaporator flask ...................................................................... 28
4.5.8
Release the evaporator flask from the vapor tube ......................................................................... 29
4.5.9
Insert the inlet tube ........................................................................................................................ 30
4.5.10
Assemble the inlet tube ................................................................................................................. 30
4.5.11
Assemble the collecting flask ......................................................................................................... 31
4.5.12
Connect the cooling medium (except G5) ...................................................................................... 31
4.5.13
Connect the vacuum ...................................................................................................................... 32
