8 meas extended measuring functions – Metrohm 796 Titroprocessor User Manual

Page 121

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7. Titration and measuring modes

796 Titroprocessor, Instructions for use

115

115

7.8 MEAS Extended measuring functions

Application:
MEAS
modes are universal measuring functions with which various meas-
urable variables of a sample can be recorded. Their features are drift or
time-controlled recording from one or more measuring points over a par-
ticular period of time.

7.8.1 Measuring modes

The following variables can be recorded:

•

potentiometric pH measurement (

MEAS_PH*)

•

potentiometric voltage measurement (

MEAS_U*)

•

amperometric measurement with polarization voltage (

MEAS_UPOL*)

•

voltametric measurement with polarization current (

MEAS_IPOL*)

In each of these measuring modes the sample solution temperature can be
determined in parallel for each measuring point and for pH measurements
the value recorded can be appropriately corrected.

•

drift or time-controlled temperature measurement (

MEAS_T*)

7.8.2 Standard measurement

The standard measurement represents a simple individual measurement
which may be drift-controlled or time-controlled. For example, in order to re-
cord the reaction behavior of a sensor it is possible to record the raw data of
the measurement at short time intervals (sampling time) and to assess them
as a measuring curve.

Note: these raw data are not exact measuring data; they are unfiltered and
influenced by the background noise of the measuring system.

The 'smoothed', i.e. filtered final measurement value (variable

CM) should

be used for calculations.

Drift / time-controlled measurement acceptance

Measurement acceptance is carried out to the same principles as in a mo-
notonic (

MET) titration. In drift-controlled measurement acceptance the

measurement drift of the sensor must be less than a defined amount in or-
der to be accepted as a valid measurement. If after a defined waiting period
has elapsed this measurement drift has not been undercut then the mo-
mentary measurement will be accepted. For time-controlled measurement
acceptance the measurement drift must be switched off. In this case only
the set waiting period is decisive for the measurement.

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