Ecd mode, Hid mode – VICI D-2-I User Manual

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18

ECD Mode

0.0

0.5

3.5

1.0

1.5

2.0

2.5

3.0

P

eak height (nA)

Length of column in detector (cm)

9.2

9.4

9.6

10.8

4.0

9.8

10.0

10.2

10.4

10.6

Detector temperature: 50 C

Working current:

15 nA

Sample:

50 ppb freon-11

2 l loop

HID Mode

0.0

0.5

3.5

1.0

1.5

2.0

2.5

3.0

P

eak height (nA)

Length of column in detector (cm)

10.6

10.8

11.0

11.2

11.4

11.6

11.8

Detector temperature: 50 C

Sample:

100 ppm n-C5

2 l loop

Figure 5: Effect of column position on detector response in ECD and HID modes

Installation

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D-2