3 grinding with liquid nitrogen, Using the device – FRITSCH PULVERISETTE 0 User Manual

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The amplitude is set manually with the Plus and Minus key on the con-

trol panel and viewed on the lid. (See Ä Chapter 6.3.1 ‘Displaying the

amplitude’ on page 25)

NOTICE!
Do not allow the grinding balls to jump too high. This can

cause damage to the lid!
Start grinding at low a amplitude and increase it slowly - do

not select an amplitude that is too high! (≤ 2 mm)

There is a risk of the grinding ball destroying the lid. The grinding stock

can be added to the mortar bowl either dry or in suspension.

CAUTION!
Do not allow any liquids to flow into the device.

To reduce the grinding noise, we recommend using a sound

absorption hood (order no. 00.0130.17).

6.1.3 Grinding with liquid nitrogen

CAUTION!
Only use grinding vessels and grinding balls made of stain-

less steel, tungsten carbide or zirconium oxide for grinding

with liquid nitrogen.

The device for grinding in liquid nitrogen (no. 00.2000.00) should be

used to embrittle the grinding stock in liquid nitrogen. In this thermally-

insulated cryo-box, the grinding vessel and the grinding ball can be

cooled down considerably, and only small amounts of liquid nitrogen

must be refilled during grinding.

Using the device

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