Metrohm 850 Professional IC Cation - Prep 2 User Manual

Page 6

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Table of contents

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IV

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850 Professional IC – Cation – Prep 2

2.14 Peristaltic pump .................................................................. 44
2.14.1

Principle of the peristaltic pump ............................................. 44

2.14.2

Installing the peristaltic pump ................................................ 45

2.15 Injection valve ..................................................................... 49
2.15.1

Connecting the injection valve ............................................... 49

2.15.2

Mode of operation of the injection valve ............................... 50

2.15.3

Selecting the sample loop ...................................................... 51

2.16 Column thermostat ............................................................ 51

2.17 Conductivity detector ......................................................... 54

2.18 Connecting the instrument ................................................ 56
2.18.1

Connecting the instrument to the PC ..................................... 56

2.18.2

Connecting the instrument to mains supply ........................... 56

2.19 Guard column ..................................................................... 57

2.20 Separation column ............................................................. 59

3 Start-up

61

3.1

Initial start-up ..................................................................... 61

3.2

Conditioning ........................................................................ 62

4 Operation and maintenance

64

4.1

General information ........................................................... 64

4.1.1

Care ...................................................................................... 64

4.1.2

Maintenance by Metrohm Service .......................................... 64

4.1.3

Operation .............................................................................. 65

4.1.4

Shutting down ...................................................................... 65

4.2

Capillary connections ......................................................... 65

4.2.1

Operation .............................................................................. 65

4.3

Door ..................................................................................... 66

4.4

Eluent ................................................................................... 66

4.4.1

Production ............................................................................. 66

4.4.2

Operation .............................................................................. 67

4.5

High pressure pump ........................................................... 67

4.5.1

Protection .............................................................................. 67

4.5.2

Maintenance ......................................................................... 68

4.6

Inline filter ........................................................................... 78

4.6.1

Maintenance ......................................................................... 78

4.7

Inline sample preparation .................................................. 80

4.8

Rinsing the sample path .................................................... 80

4.9

Sample degasser ................................................................. 82

4.9.1

Operation .............................................................................. 82

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