Waters Sep-Pak DNPH-Silica Cartridges - Manual

[ Care and Use ManUal ]
Waters Sep-Pak DNPH-Silica Cartridge
1
Contents
I. IntroduCtIon
a. Sep-Pak DNPH-Silica Cartridge Description
II. usInG seP-PAK dnPH CArtrIdGes
a. Theory of Operation
b. Preventing Contamination
c. Collecting the Sample
d. Eluting the Derivatives
III. AnALYZInG tHe dnPH derIVAtIVes
a. Operating Guidelines
b. Performing HPLC Analysis
c. Analyzing a Cartridge Blank
d. Selecting Separation Conditions
IV. APPLICAtIon eXAMPLes
a. Estimating Sample Volume
b. Analysis of Auto Exhaust Emissions
c. Analysis of Residential Air
d. Analysis of Research Lab Air
V. storAGe And dIsPosAL oF used CArtrIdGes
VI. trouBLesHootInG
VII. reFerenCes And BIBLIoGrAPHY
VIII. orderInG InForMAtIon APPendICes
IX. APPendICes
a. Measuring Acetonitrile Purity
b. Synthesizing DNPH Derivative Standards
c. Measuring Sample Breakthrough
I. IntroduCtIon
Waters Sep-Pak ® DNPH-Silica cartridges are convenient, reproducible
sampling devices for quantifying aldehydes and ketones in gasses,
including air within a range of 1 to 5,000 parts per billion (ppbv).
WAters seP-PAK dnPH-sILICA CArtrIdGe