Labconco FreeZone 4.5 Liter Freeze Dry Systems 77510 Series User Manual
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CHAPTER 1: INTRODUCTION
1
Freeze Dry Process
1
Freeze Dry Rates
1
Freeze Dry Capacity
3
Samples Containing Volatile Substances
4
About This Manual
4
Typographical Conventions
5
Your Next Step
5
CHAPTER 2: PREREQUISITES
6
Electrical Requirements
6
Location Requirements
6
Vacuum Pump Requirements
7
Chamber or Manifold Requirements
7
CHAPTER 3: GETTING STARTED
8
Unpacking Your Freeze Dryer
8
Freeze Dryer Components
9
Setting Up Your Freeze Dryer
10
Component Orientation
10
Vacuum Pump Connection
11
Electrical Connection
11
Chemical Resistance of Freeze Dryer Components
11
Solvent Safety Precautions
13
CHAPTER 4: USING YOUR FREEZE DRYER
14
Freeze Dryer Controls
15
Operation Checklist
16
Vacuum Pump Ballast Setting
16
Operating the Freeze Dryer
16
Set-Up
16
Automatic Start-Up
18
Manual Start-Up
18
Setting the Operating Vacuum Level
19
Pre-Freezing Samples
19
Adding Sample
20