2 systematic error diagnostics, Systematic error diagnostics, 9 systematic error diagnostics – Metrohm 896 Professional Detector – Conductivity & Amperometry User Manual

Page 50

Advertising
background image

6.9 Systematic error diagnostics

■■■■■■■■■■■■■■■■■■■■■■

42

■■■■■■■■

2.896.0030 896 Professional Detector – Conductivity & Amperometry

6.9

Systematic error diagnostics

If the causes of a malfunction cannot be found among the problem
descriptions in the above chapters, then proceed systematically as follows:

Systematic error diagnostics

1 Restarting the instrument and the software

■

Switch off the instrument.

■

Close and restart MagIC Net™.

■

Switch the instrument back on again.

If the problem has not yet been localized, continue with Step 2.

2 Performing instrument test with dummy cell

(see Chapter 4.1, page 20)

If the problem has not yet been localized, continue with Step 3.

3 Checking software settings

■

Check the method parameters of the detector and reset them to
values that you know will function.

■

Check the measuring range and reset it to values that you know
will function or select a larger measuring range.

■

Check manual changes to the settings and reset them to values
that you know will function.

■

Check manual settings in the time program and reset them to val-
ues that you know will function.

If the problem has not yet been localized, continue with Step 4.

4 Cleaning the measuring cell

■

Switch off the measuring cell.

■

Remove the measuring cell.

■

Clean the measuring cell (see measuring cell manual).

■

Polish the working electrode (see the leaflet for the working elec-
trode).

■

Reinsert the measuring cell.

If the problem has not yet been localized, continue with Step 5.

5 Replacing the reference electrode

If the problem has not yet been localized, continue with Step 6.

Advertising