Metrohm 850 Professional IC Anion MSM-HC MCS Prep 1 - Manual (Page 123)

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6 Troubleshooting
850 Professional IC – Anion MSM-HC – MCS – Prep 1
￭￭￭￭￭￭￭￭ 113
Problem Cause Remedy
￭ Replace separation column (see "Connect-
ing and rinsing the separation column",
page 75).
Conductivity detec-
tor is not recognized
in the software No connection.
￭ Check the cable connection (37- 1 ).
￭ Turn the instrument off and on again (after
15 seconds).
Extreme spread of
the peaks in the
chromatogram.
Splitting (dual
peaks) Connections – dead vol-
ume in the system. Check the connections (see Chapter 3.5, page
24) (use PEEK capillaries with an internal diam-
eter of 0.25 mm between the injection valve
and detector).
Guard column – diminished
performance. ￭ Replace guard column (see Chapter 3.21,
page 72).
Separation column – dead
volume at column head. ￭ Install separation column in reverse flow
direction (if permitted by the information
sheet).
￭ Replace separation column (see "Connect-
ing and rinsing the separation column",
page 75).
Greater rise in the
baseline MSM-HC – reduced
capacity. Regenerate the MSM-HC (see Chapter
5.11.3.1, page 98).
Precision problems -
significant scatter-
ing of the measured
values Sample – Gas bubbles in
the sample. Use sample degasser (see Chapter 3.13, page
50).
Injection valve – sample
loop. Check installation of the sample loop (see
Chapter 3.14.1, page 51).
Sample – Rinsing volume
too low. Prolong the rinsing time (see Chapter 5.8,
page 95).
Injection valve – defective. Request Metrohm Service.
MCS – vacuum too low. ￭ Check connectors. If they are ok:
￭ Contact the Metrohm Service.
Unexpected change
to the retention
times in the chroma-
tograms Separation column –
diminished separating effi-
ciency. ￭ Regenerate separation column (see Chap-
ter 5.15.4, page 108).
￭ Replace separation column (see "Connect-
ing and rinsing the separation column",
page 75).