Labconco FreeZone Triad Freeze Dry System 74000 Series User Manual

Page 3

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T

T

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A

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B

L

L

E

E

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O

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F

C

C

O

O

N

N

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N

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CHAPTER 1: INTRODUCTION

1

Freeze Dry Process

1

Freeze Dry Rates

2

Freeze Dry Capacity

3

Samples Containing Volatile Substances

3


CHAPTER 2: PREREQUISITES

5

Electrical Requirements

5

Location Requirements

5

Vacuum Pump Requirements

6


CHAPTER 3: GETTING STARTED

7

Unpacking Your Triad Freeze Dry

7

Triad Freeze Dry Components

8

Setting Up Your Triad Freeze Dry System

8

Component Orientation and Hose Connection

8

Venting the Vacuum Pump

9

Electrical Connection

9

Chemical Resistance of Freeze Dryer Components

9

Solvent Safety Precautions

11


CHAPTER 4: OPERATING INSTRUCTION

12

Triad Freeze Dry Controls

13

Operation Checklist

14

Vacuum Pump Ballast Setting

14

Operating the Triad Freeze Dry System

15

Set-Up

15

Setting the Operating Vacuum Level

17

Manual Control Operation

18

Automatic Control Operation

19

Programming

20

Starting the Freeze Dry Cycle

21

Changing the Program Parameters in the Middle of a Run

22

Stopping the Freeze Dry Cycle

22

Monitoring the system Operation

23

Sample Freezing

23

Shelf Loading

23

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