Method 3, Method 4 – Metrohm 813 Compact Autosampler User Manual

Page 32

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3.4 The methods

26

813 Compact Autosampler

Method 3

(detailed command sequence, see 4.2 Sequences)

Double determination of each sample, no air gap, needle remains

in sample after sample transfer.

Sequence:

1. Await first Remote signal of the instrument.
2. Get sample tube and immerse needle.
3. On receiving second Remote signal, switch on the peristaltic

pump. Sample is transferred.

4. Await third Remote signal. The instrument starts its determi-

nation.

5. Peristaltic pump is switched off after 12 s.
6. Await first Remote signal of the instrument again.
7. On receiving second Remote signal, switch on the peristaltic

pump. Sample is transferred.

8. Await third Remote signal. The starts the second determina-

tion.

9. Peristaltic pump is switched off after 12 s.

Method 4

(detailed command sequence, see 4.2 Sequences)

Triple determination of each sample, no air gap, needle remains in

sample after sample transfer.

Sequence:

1. Await first Remote signal of the instrument.
2. Get sample tube and immerse needle.
3. On receiving second Remote signal, switch on the peristaltic

pump. Sample loop is transferred.

4. Await third Remote signal. The instrument starts its determi-

nation.

5. Peristaltic pump is switched off after 12 s.
6. Await first Remote signal of the instrument again.
7. On receiving second Remote signal, switch on the peristaltic

pump. Sample is transferred.

8. Await third Remote signal. The instrument starts the second

determination.

9. Peristaltic pump is switched off after 12 s.
10. Await first Remote signal of the IC again.
11. On receiving second Remote signal, switch on the peristal-

tic pump. Sample is transferred.

12. Await third Remote signal. The instrument starts the third

determination.

13. Peristaltic pump is switched off after 12 s.

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