Metrohm NIRS XDS SmartProbe Analyzer - Manual (Page 63)

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The Number of Samples should be 10, as shown.
The wavelength standard for reflectance is the
SRM-1920 plus talc. This is the same cell used for
Instrument Calibration.
Current versions of Vision default to this
selection, for this instrument. Please verify that it
is correct.
Click “OK” when ready.
Vision requests that the user place the instrument reference into
position. This is automatic with the Smart Probe Analyzer; no response
is required.
When the reference scan is finished, insert the
wavelength standard as directed.
Always place the standard into the instrument in the
same orientation. In this case, the user has marked
the standard for repeatable positioning.
Click “OK” when ready.
When the test is complete, a spectrum of the standard is shown in the upper right quadrant of the
screen. A tabular report is shown in the lower right quadrant, giving each peak, its nominal position
and its measured position. The difference from nominal, and the repeatability of wavelength peak
positions are calculated.