4 using the external keyboard, 2 melting point determination, 1 sample preparation – BUCHI Melting Point M-565 User Manual

Page 26: 4 using the external keyboard 6.2, Melting point determination, 6 .2 melting point determination

Advertising
background image

6 Operation

26

Melting Point M-565 Operation Manual, Version D

6 .1 .4

Using the external keyboard

NOTE
The instrument can be operated using an external keyboard.

For the softkeys, the following keys of the external keyboard are assigned:
• ENTER = right softkey
• Alt = center softkey
• Esc = left softkey
• In the method menu: To navigate quickly to a method name press the initial letter.

6 .2

Melting point determination

NOTE
For exact melting point determination, use original capillaries from BUCHI only. If other capillaries are
used, the results can be wrong. Use the following items:

Product

Order number

Melting point capillaries, 100 units

017808

Melting point capillaries, 1000 units

001759

Fig. 6.1: Melting point capillaries

6 .2 .1

Sample preparation

NOTE
Use only capillaries from BUCHI. They are precise and adequate for this kind of operation. Other
capillaries have other dimensions and wall thicknesses. Using others may result in results that are
incorrect.

Each sample has to be prepared.
The following methods to compact the samples are recommended:
• Using the Sample Loader M-569
• Knocking the capillaries on a hard surface.

NOTE
Sample preparation by letting the capillaries fall through a tube is not advised, because cross
contamination may occur.

Advertising