3uhsdudwlrq dqg &duu\lqj 2xw 0hdvxuhphqwv – IKA C 7000 Grundausstattung Set 2 User Manual

Page 39

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IKA

-WERKE C 7000

Ver. 07 09.07

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The term "measurements" as used here means both measurements for calibrating

the instrument (calibration measurements) and measurements made to determine a

gross calorific value. The difference lies mainly in the evaluation of the results,

preparation and execution are almost identical for both types of measurement.

A complete test procedure comprises the following operations and procedures (for

detailed information about the individual steps, please see further sections in this

chapter):

c

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For example, homogenise sample material, press to form pellets, dry

d

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Weigh the sample in a crucible to an accuracy of 0.1 mg

e

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Place the sample in the decomposition vessel and close the vessel .

f

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Fill the decomposition vessel manually with oxygen at 30 bar, quality 3.5, using the

IKA

C 48 oxygen filling station.

5.M easurem ent

6.C ooling

7.Vent

8.C lean

1.Prepare

sam ple

3.Place

sam ple

4.Fill with

oxygen

2. W eigh

'9 1R 

'9 1R 

'9 1R 

'9 1R 

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