Metrohm 848 Titrino plus - Manual (Page 7)

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Table of contents
848 Titrino plus
￭￭￭￭￭￭￭￭ V
6.6 Configuring external devices ............................................. 63
6.7 Instrument diagnosis .......................................................... 66
6.7.1 Loading program versions and language files ......................... 66
6.7.2 Diagnosis functions ............................................................... 67
7 Parameters 68
7.1 Dynamic equivalence point titrations (DET) ..................... 68
7.1.1 Start conditions ..................................................................... 68
7.1.2 Titration parameters .............................................................. 69
7.1.3 Stop conditions ..................................................................... 74
7.1.4 Evaluation ............................................................................. 76
7.1.5 Calculation ............................................................................ 79
7.1.6 Statistics ................................................................................ 81
7.1.7 Reports .................................................................................. 81
7.2 Monotonic equivalence point titrations (MET) ................ 83
7.2.1 Start conditions ..................................................................... 83
7.2.2 Titration parameters .............................................................. 84
7.2.3 Stop conditions ..................................................................... 89
7.2.4 Evaluation ............................................................................. 90
7.2.5 Calculation ............................................................................ 93
7.2.6 Statistics ................................................................................ 95
7.2.7 Reports .................................................................................. 95
7.3 Endpoint titrations (SET) .................................................... 97
7.3.1 Conditioning ......................................................................... 97
7.3.2 Start conditions ..................................................................... 98
7.3.3 Titration parameters ............................................................ 100
7.3.4 Control parameters EP1 ....................................................... 102
7.3.5 Control parameters EP2 ....................................................... 105
7.3.6 Stop conditions ................................................................... 105
7.3.7 Calculation .......................................................................... 106
7.3.8 Statistics .............................................................................. 108
7.3.9 Reports ................................................................................ 108
7.4 pH calibration (CAL) ......................................................... 110
7.4.1 Calibration parameters ........................................................ 110
7.4.2 Buffers ................................................................................. 112
7.4.3 Reports ................................................................................ 113
8 Operation and maintenance 114
8.1 Quality Management and validation with Metrohm .... 114
9 Troubleshooting 115
9.1 SET titration ...................................................................... 115
9.2 Miscellaneous ................................................................... 116