Metrohm 886 Prof.Thermostat/Reactor - Manual (Page 33)

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation
886 Professional Thermostat (2.886.0110) / 886 Professional Reactor (2.896.0210) ￭￭￭￭￭￭￭￭ 25
3 Reactor outlet capillary
Section of PEEK capillary (6.1831.100) or the
PTFE capillary (6.1803.150)
*
4 Reagent inlet capillary
Section of PEEK capillary (6.1831.100)
5 Backpressure column
Metrosep BP 1 Guard/2.0 (6.1015.100)
* In bromate determination with the tri-iodide method, the tri-iodide is
partially absorbed by the PEEK capillary, which leads to peak widening and
a lower detection limit. Therefore, for this application, we recommend to
use the PTFE capillary (6.1803.150).
To connect the capillaries, you need the following accessories:
￭ the long PEEK capillary (6.1831.100)
￭ the capillary cutter (6.2621.080)
￭ If the reagent is delivered via high pressure pump: the backpressure
column 6.1015.100 Metrosep BP 1 Guard/2.0
1 Connect the reactor inlet capillary
￭ Attach the column outlet capillary (13-1) to one of the two Y con-
nector inlets.
￭ Connect the Y connector output and reactor input with a short
section of the 6.1831.100 PEEK capillary (13-2).
2 Connect the reagent inlet capillary
￭ For reagent delivery, attach a section of the 6.1831.100 PEEK
capillary to the second Y connector inlet.
￭ Attach the backpressure column (13-5) at he other end.
￭ Attach another section of the 6.1831.100 PEEK capillary to the
other end of the backpressure column (13-4).
3 Connect the reactor outlet capillary
￭ Attach a section of the 6.1831.100 PEEK capillary (13-3) at the
reactor output.
Inserting the reactor plate (6.2845.100)
To insert the reactor plate, you need the 6.2621.140 hexagon key 2.5
mm.